Valyllysine

Base Information

Chemical Name:Valyllysine
CAS No.:22677-62-9
Molecular Formula:C11H23 N3 O3
Molecular Weight:245.322
Hs Code.:2924199090
UNII:02GD87WMPH
DSSTox Substance ID:DTXSID80177209
Nikkaji Number:J1.316.520C
Wikidata:Q27145073
Metabolomics Workbench ID:79047
Mol file:22677-62-9.mol

Synonyms:Val-Lys;valyl-lysine;valyllysine

Suppliers and Price of Valyllysine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 8 raw suppliers

Chemical Property of Valyllysine

Chemical Property:

Vapor Pressure:1.81E-10mmHg at 25°C
Boiling Point:478.4°Cat760mmHg
PKA:3.09±0.10(Predicted)
Flash Point:243.1°C
PSA：121.93000
Density:1.119g/cm³
LogP:1.90900
XLogP3:-3.6
Hydrogen Bond Donor Count:4
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:8
Exact Mass:245.17394160
Heavy Atom Count:17
Complexity:256

Purity/Quality:: 98%Min ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(C)C(C(=O)NC(CCCCN)C(=O)O)N
Isomeric SMILES:CC(C)[C@@H](C(=O)N[C@@H](CCCCN)C(=O)O)N

Technology Process of Valyllysine

There total 8 articles about Valyllysine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: benzyl N₆-((benzyloxy)carbonyl)-N₂-(((benzyloxy)carbonyl)-L-valyl)-L-lysinate

: 22677-62-9
L-valyl-L-lysine

Guidance literature:: With palladium on carbon; hydrogen; In methanol; water; for 72h;

Reference yield:

: 2486-81-9
Z-Val-Lys<(N^ε)Z>-OH

: 22677-62-9
L-valyl-L-lysine

Guidance literature:: With hydrogenchloride; hydrogen; palladium; In methanol;
DOI:10.1246/bcsj.37.1809

Reference yield:

: 1149-26-4
(S)-N-(benzyloxycarbonyl)valine

: 22677-62-9
L-valyl-L-lysine

Guidance literature:: Multi-step reaction with 3 steps

1: (i) ClCO₂iBu, Et₃N, toluene, (ii) /BRN= 3578476/, CHCl₃

2: aq. NaOH / dioxane

3: H₂, aq. HCl / Pd / methanol

With hydrogenchloride; sodium hydroxide; hydrogen; palladium; In 1,4-dioxane; methanol;
DOI:10.1246/bcsj.37.1809