1-Methyl-3-(((triphenylphosphoranylidene)amino)carbonyl)pyridinium iodide

Base Information

Chemical Name:1-Methyl-3-(((triphenylphosphoranylidene)amino)carbonyl)pyridinium iodide
CAS No.:125583-35-9
Molecular Formula:C₂₅H₂₂N₂OP*I
Molecular Weight:524.341
Hs Code.:
DSSTox Substance ID:DTXSID30925176
Mol file:125583-35-9.mol

Synonyms:125583-35-9;1-Methyl-3-(((triphenylphosphoranylidene)amino)carbonyl)pyridinium iodide;Pyridinium, 1-methyl-3-(((triphenylphosphoranylidene)amino)carbonyl)-, iodide;1-methyl-N-(triphenyl-lambda5-phosphanylidene)pyridin-1-ium-3-carboxamide;iodide;Pyridinium, 1-methyl-3-(((triphenylphosphoranylidene)amino)carbonyl)-, iodide;C25H22N2OP.I;DTXSID30925176;OZBXMACVDMGHHH-UHFFFAOYSA-M;C25-H22-N2-O-P.I;LS-132788;1-Methyl-3-[(triphenyl-lambda~5~-phosphanylidene)carbamoyl]pyridin-1-ium iodide

Suppliers and Price of 1-Methyl-3-(((triphenylphosphoranylidene)amino)carbonyl)pyridinium iodide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
PYRIDINIUM, 1-METHYL-3-(((TRIPHENYLPHOSPHORANYLIDENE)AMINO)CARBONYL)-, IODIDE 95.00%
5MG
$ 504.48

Total 3 raw suppliers

Chemical Property of 1-Methyl-3-(((triphenylphosphoranylidene)amino)carbonyl)pyridinium iodide

Chemical Property:

PSA：43.12000
LogP:0.83300
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:4
Exact Mass:524.05145
Heavy Atom Count:30
Complexity:533

Purity/Quality:

98%min ^*data from raw suppliers

PYRIDINIUM, 1-METHYL-3-(((TRIPHENYLPHOSPHORANYLIDENE)AMINO)CARBONYL)-, IODIDE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C[N+]1=CC=CC(=C1)C(=O)N=P(C2=CC=CC=C2)(C3=CC=CC=C3)C4=CC=CC=C4.[I-]

Technology Process of 1-Methyl-3-(((triphenylphosphoranylidene)amino)carbonyl)pyridinium iodide

There total 3 articles about 1-Methyl-3-(((triphenylphosphoranylidene)amino)carbonyl)pyridinium iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 125583-34-8
N-(3-pyridylcarbonyl)triphenylphospha-λ⁵-azene

: 74-88-4
methyl iodide

: 125583-35-9
N-(10methylpyridinium-3-carbo)iminotriphenylphosphine

Guidance literature:: In ethanol; for 2h;
DOI:10.1007/BF00764439

Reference yield:

: 98-92-0,1255150-40-3
nicotinamide

: 125583-35-9
N-(10methylpyridinium-3-carbo)iminotriphenylphosphine

Guidance literature:: Multi-step reaction with 3 steps

1: tert-butyl hypochlorite / CCl₄ / 60 - 70 °C

2: 76 percent / Et₃N / benzene / Heating

3: 83 percent / ethanol / 2 h

With tert-butylhypochlorite; triethylamine; In tetrachloromethane; ethanol; benzene;
DOI:10.1007/BF00764439

Reference yield:

: 63458-55-9
N-monochloronicotinamide

: 125583-35-9
N-(10methylpyridinium-3-carbo)iminotriphenylphosphine

Guidance literature:: Multi-step reaction with 2 steps

1: 76 percent / Et₃N / benzene / Heating

2: 83 percent / ethanol / 2 h

With triethylamine; In ethanol; benzene;
DOI:10.1007/BF00764439