Diethyl(2-methyl-3-phenylaziridin-1-yl)phosphonate

Base Information

Chemical Name:Diethyl(2-methyl-3-phenylaziridin-1-yl)phosphonate
CAS No.:80252-32-0
Molecular Formula:C₁₃H₂₀NO₃P
Molecular Weight:269.28
Hs Code.:
NSC Number:138173
DSSTox Substance ID:DTXSID70300665

Synonyms:80252-32-0;diethyl(2-methyl-3-phenylaziridin-1-yl)phosphonate;NSC138173;DTXSID70300665;NSC-138173

Suppliers and Price of Diethyl(2-methyl-3-phenylaziridin-1-yl)phosphonate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of Diethyl(2-methyl-3-phenylaziridin-1-yl)phosphonate

Chemical Property:

Vapor Pressure:7.65E-05mmHg at 25°C
Boiling Point:342.2°C at 760 mmHg
Flash Point:160.8°C
Density:1.15g/cm³
XLogP3:2.2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:6
Exact Mass:269.11808050
Heavy Atom Count:18
Complexity:307

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCOP(=O)(N1C(C1C2=CC=CC=C2)C)OCC

Technology Process of Diethyl(2-methyl-3-phenylaziridin-1-yl)phosphonate

There total 4 articles about Diethyl(2-methyl-3-phenylaziridin-1-yl)phosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.5%

: 80252-19-3,80252-20-6
erythro-diethyl N-(β-bromo-β-phenylpropyl)phosphoroamidate

: 30616-11-6,80252-32-0
trans-N-(diethoxyphosphoryl)-2-methyl-3-phenylaziridine

Guidance literature:: With sodium ethanolate; In dichloromethane; for 1h; Ambient temperature;
DOI:10.1016/S0040-4020(01)98974-4

Reference yield:

: 873-66-5
1-propenylbenzene

: 30616-11-6,80252-32-0
trans-N-(diethoxyphosphoryl)-2-methyl-3-phenylaziridine

Guidance literature:: Multi-step reaction with 2 steps

1: 2.) aq. sodium bisulphite / 1.) dichloromethane, reflux, 1 h 2.) 10 deg C

2: 97.5 percent / sodium ethoxide / CH₂Cl₂ / 1 h / Ambient temperature

With sodium ethanolate; sodium hydrogensulfite; In dichloromethane;
DOI:10.1016/S0040-4020(01)98974-4

Reference yield:

: 766-90-5
cis-1-phenyl-1-propylene

: 30616-11-6,80252-32-0
trans-N-(diethoxyphosphoryl)-2-methyl-3-phenylaziridine

Guidance literature:: Multi-step reaction with 2 steps

1: 2.) aq. sodium bisulphite / 1.) dichloromethane, reflux, 1 h 2.) 10 deg C

2: 97.5 percent / sodium ethoxide / CH₂Cl₂ / 1 h / Ambient temperature

With sodium ethanolate; sodium hydrogensulfite; In dichloromethane;
DOI:10.1016/S0040-4020(01)98974-4