3,5-Dimethyl-4-(phenylazo)thiopyrazole-1-carboxamide

Base Information

Chemical Name:3,5-Dimethyl-4-(phenylazo)thiopyrazole-1-carboxamide
CAS No.:3696-00-2
Molecular Formula:C12H13N5S
Molecular Weight:259.335
Hs Code.:
NSC Number:127101

Synonyms:F 2354;NSC 127101;BRN 0751738;3,5-Dimethyl-4-(phenylazo)thiopyrazole-1-carboxamide;3696-00-2;Pyrazole-1-carboxamide, 3,5-dimethyl-4-(phenylazo)thio-;4-Phenylazo-3,5-dimethyl-pyrazol-1-thiocarbonsaeureamid [German];5-25-18-00095 (Beilstein Handbook Reference);4-Phenylazo-3,5-dimethyl-pyrazol-1-thiocarbonsaeureamid;NSC127101;NSC-127101;LS-128195

Suppliers and Price of 3,5-Dimethyl-4-(phenylazo)thiopyrazole-1-carboxamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of 3,5-Dimethyl-4-(phenylazo)thiopyrazole-1-carboxamide

Chemical Property:

Vapor Pressure:3.61E-09mmHg at 25°C
Boiling Point:474.4°C at 760 mmHg
Flash Point:240.7°C
Density:1.31g/cm³
XLogP3:2.7
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:2
Exact Mass:259.08916661
Heavy Atom Count:18
Complexity:326

Purity/Quality:: 95% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=C(C(=NN1C(=S)N)C)N=NC2=CC=CC=C2

Technology Process of 3,5-Dimethyl-4-(phenylazo)thiopyrazole-1-carboxamide

There total 3 articles about 3,5-Dimethyl-4-(phenylazo)thiopyrazole-1-carboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 123-54-6,81235-32-7
acetylacetone

: 3696-00-2
3,5-dimethyl-4-phenylazo-N-thiocarbomylpyrazole

Guidance literature:: Multi-step reaction with 2 steps

1: cis-nitrous acid / 0 - 5 °C

2: ethanol / Reflux

With cis-nitrous acid; In ethanol;
DOI:10.1371/journal.pone.0196016

Reference yield:

: 62-53-3
aniline

: 3696-00-2
3,5-dimethyl-4-phenylazo-N-thiocarbomylpyrazole

Guidance literature:: Multi-step reaction with 2 steps

1: cis-nitrous acid / 0 - 5 °C

2: ethanol / Reflux

With cis-nitrous acid; In ethanol;
DOI:10.1371/journal.pone.0196016