1-(2-hydroxyethyl)-2-methyl-5-aminoimidazole

Base Information

• Chemical Name: 1-(2-hydroxyethyl)-2-methyl-5-aminoimidazole
• CAS No.: 84145-87-9
• Molecular Formula: C6H11 N3 O
• Molecular Weight: 141.173
• Hs Code.: 2933290090
• Mol file: 84145-87-9.mol

Synonyms:1-(2-Hydroxyethyl)-2-methyl-5-aminoimidazole;5-Amino-1-(2-hydroxyethyl)-2-methylimidazole

Chemical Property of 1-(2-hydroxyethyl)-2-methyl-5-aminoimidazole

Chemical Property:

• Vapor Pressure: 4.62E-07mmHg at 25°C
• Boiling Point: 398.4°C at 760 mmHg
• Flash Point: 194.7°C
• PSA: 64.07000
• Density: 1.29g/cm³
• LogP: 0.34720

Purity/Quality:

98% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1-(2-hydroxyethyl)-2-methyl-5-aminoimidazole

There total 2 articles about 1-(2-hydroxyethyl)-2-methyl-5-aminoimidazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

metronidazole (443-48-1) → 2-(5-amino-2-methyl-1H-imidazol-1-yl)ethan-1-ol (84145-87-9)

Guidance literature:

With palladium on carbon (10%); In 1,4-dioxane; at 20 ℃; for 6h; Cooling with ice; Inert atmosphere;

Reference yield:

metronidazole (443-48-1) → 2-methyl-5-nitro-1H-imidazole (696-23-1,88054-22-2) + 2-(5-amino-2-methyl-1H-imidazol-1-yl)ethan-1-ol (84145-87-9) + N-(2'-hydroxyethyl)-2-methylimidazole (1615-15-2)

Guidance literature:

With sodium tetrahydroborate; iron; at 25 ℃; pH=7;

DOI:10.1016/j.molliq.2016.10.040

Reference yield: 87.0%

1-Phenyl-4,4,4-trifluorobutane-1,3-dione (326-06-7) + 2-(5-amino-2-methyl-1H-imidazol-1-yl)ethan-1-ol (84145-87-9) → 2-[2-methyl-5-phenyl-7-(trifluoromethyl)-3H-imidazo[4,5-b]pyridin-3-yl]ethanol

Guidance literature:

In dichloromethane; Inert atmosphere; Reflux;

DOI:10.1055/s-0029-1216802

upstream raw materials:

metronidazole

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