2-Acetylpyridine semicarbazone

Base Information

Chemical Name:2-Acetylpyridine semicarbazone
CAS No.:14534-93-1
Molecular Formula:C8H10 N4 O
Molecular Weight:178.19
Hs Code.:2933990090
ChEMBL ID:CHEMBL1099026
Mol file:14534-93-1.mol

Synonyms:2-acetylpyridine semicarbazone;APSC

Suppliers and Price of 2-Acetylpyridine semicarbazone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of 2-Acetylpyridine semicarbazone

Chemical Property:

Boiling Point:°Cat760mmHg
Flash Point:°C
PSA：80.37000
Density:1.27g/cm³
LogP:1.56510
XLogP3:0.1
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:2
Exact Mass:178.08546096
Heavy Atom Count:13
Complexity:214

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(=NNC(=O)N)C1=CC=CC=N1
Isomeric SMILES:C/C(=N\NC(=O)N)/C1=CC=CC=N1

Technology Process of 2-Acetylpyridine semicarbazone

There total 1 articles about 2-Acetylpyridine semicarbazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 1122-62-9
2-acetylpyridine

: 563-41-7
semicarbazide hydrochloride

: 14534-93-1
2-acetylpyridine semicarbazone

Guidance literature:: With sodium acetate; In water; for 2h;
DOI:10.1155/2014/616459

Reference yield: 81.0%

: 14534-93-1
2-acetylpyridine semicarbazone

: 5419-55-6
Triisopropyl borate

: 98-05-5
phenylarsonic acid

: C₆H₅AsO₃B(C₅H₄NC(CH₃)NNCONH₂)

Guidance literature:: In benzene; byproducts: HOCH(CH3)2; refluxing phenylarsonic acid and B-compd. in dry benzene for 10-12 h under anhyd. conditions, addn. of ligand, refluxing again until all isopropanol is liberated; removal of solvent over the ratio head, drying under reduced pressure, washing with n-hexane and benzene, elem. anal.;

Reference yield: 77.0%

: 14534-93-1
2-acetylpyridine semicarbazone

: 98-80-6
phenylboronic acid

: C₆H₅B(OC(NH₂)NNC(CH₃)C₅H₄N)2

Guidance literature:: In benzene; byproducts: H2O; refluxing for 8-12 h with monitoring of H2O liberation; distn., drying in vac., washing (cyclohexane), drying (2 h), elem. anal.;