CID 6331469

Base Information

• Chemical Name: CID 6331469
• CAS No.: 5715-80-0
• Molecular Formula: C11H13N2NaS2
• Molecular Weight: 260.359
• Mol file: 5715-80-0.mol

Synonyms:

Chemical Property of CID 6331469

Chemical Property:

• Vapor Pressure: 1.99E-05mmHg at 25°C
• Boiling Point: 362°C at 760 mmHg
• Flash Point: 172.7°C
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 1
• Exact Mass: 261.04961008
• Heavy Atom Count: 16
• Complexity: 219

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1CN(CCN1C2=CC=CC=C2)C(=S)S.[Na]

Technology Process of CID 6331469

There total 1 articles about CID 6331469 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

carbon disulfide (75-15-0,12122-00-8) + 4-phenyl-1-piperazine (92-54-6) → sodium 4-phenylpiperazine-1-carbodithioate (5715-80-0)

Guidance literature:

With sodium hydroxide; In methanol; at 0 - 4 ℃; for 4h;

DOI:10.1016/j.molstruc.2018.05.068

Reference yield: 94.5%

N-(9-acridinyl)-2-chloroacetamide (100954-63-0) + sodium 4-phenylpiperazine-1-carbodithioate (5715-80-0) → 2-(9-acridinylamino)-2-oxoethyl 4-phenylpiperazine-1-carbodithioate

Guidance literature:

In acetone; for 8h; Reflux;

DOI:10.3390/molecules23082033

Reference yield: 90.0%

uranium oxide chloride + sodium 4-phenylpiperazine-1-carbodithioate (5715-80-0) → UO2(C6H5C4H8N2CS2)2 (114075-44-4)

Guidance literature:

In ethanol; water; stirring (room temp.); washing (H2O, MeOH, Et2O), drying; elem. anal.;

DOI:10.1080/00945719809349365

upstream raw materials:

carbon disulfide

4-phenyl-1-piperazine

Downstream raw materials:

UO₂(C₆H₅C₄H₈N₂CS₂)2

bis(4-phenylpiperazine-1-carbodithioato)cobalt(II)

phenylpiperazyldithiocarbamato-S,S' copper(II)