6-(3-Nitrophenyl)-4,5-dihydropyridazin-3(2h)-one

Base Information

Chemical Name:6-(3-Nitrophenyl)-4,5-dihydropyridazin-3(2h)-one
CAS No.:52239-76-6
Molecular Formula:C10H9N3O3
Molecular Weight:219.2
Hs Code.:
NSC Number:162059
DSSTox Substance ID:DTXSID10303791
Wikidata:Q82049253
Mol file:52239-76-6.mol

Synonyms:6-(3-nitrophenyl)-4,5-dihydropyridazin-3(2h)-one;52239-76-6;NSC162059;SCHEMBL11624623;DTXSID10303791;STL572863;AKOS016373581;NSC-162059

Suppliers and Price of 6-(3-Nitrophenyl)-4,5-dihydropyridazin-3(2h)-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of 6-(3-Nitrophenyl)-4,5-dihydropyridazin-3(2h)-one

Chemical Property:

Density:1.47g/cm³
XLogP3:0.8
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:1
Exact Mass:219.06439116
Heavy Atom Count:16
Complexity:335

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1CC(=O)NN=C1C2=CC(=CC=C2)[N+](=O)[O-]

Technology Process of 6-(3-Nitrophenyl)-4,5-dihydropyridazin-3(2h)-one

There total 4 articles about 6-(3-Nitrophenyl)-4,5-dihydropyridazin-3(2h)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 6328-00-3
4-(3-nitro-phenyl)-4-oxo-butyric acid

: 52239-76-6
3-(m-Nitrophenyl)-6-oxo-1,4,5,6-tetrahydropyridazine

Guidance literature:: With potassium hydroxide; hydrazine hydrochloride; In water; for 2h; Heating;
DOI:10.1007/BF00522738

Reference yield:

: 90991-20-1
4-(3-nitro-phenyl)-4-oxo-butyric acid methyl ester

: 52239-76-6
3-(m-Nitrophenyl)-6-oxo-1,4,5,6-tetrahydropyridazine

Guidance literature:: With hydrazine hydrate; In methanol;
DOI:10.1016/0960-894X(95)00577-G

Reference yield:

: 2051-95-8
succinylbenzene

: 52239-76-6
3-(m-Nitrophenyl)-6-oxo-1,4,5,6-tetrahydropyridazine

Guidance literature:: Multi-step reaction with 3 steps

1: HNO₃ fuming

2: BF₃*Et₂O

3: NH₂NH₂*H₂O / methanol

With boron trifluoride diethyl etherate; nitric acid; hydrazine hydrate; In methanol;
DOI:10.1016/0960-894X(95)00577-G