N,N-bis(prop-2-en-1-yl)acetamide

Base Information

• Chemical Name: N,N-bis(prop-2-en-1-yl)acetamide
• CAS No.: 6296-61-3
• Molecular Formula: C8H13NO
• Molecular Weight: 139.197
• NSC Number: 54289,48108
• DSSTox Substance ID: DTXSID60978817
• Nikkaji Number: J1.106.988F
• Wikidata: Q82964303
• Mol file: 6296-61-3.mol

Synonyms:N,N-Diallylacetamide;N,N-bis(prop-2-en-1-yl)acetamide;6296-61-3;N,N-bis(prop-2-enyl)acetamide;Acetamide, N,N-di-2-propenyl-;N-acetyldiallylamine;NSC48108;N,N-diallyl-acetamide;SCHEMBL173228;DTXSID60978817;BGQJNGISTPIALH-UHFFFAOYSA-N;ADAL1243799;N,N-Di(prop-2-en-1-yl)acetamide;NSC54289;NSC-48108;NSC-54289;AKOS003847006;EN300-188024

Chemical Property of N,N-bis(prop-2-en-1-yl)acetamide

Chemical Property:

• Vapor Pressure: 0.256mmHg at 25°C
• Boiling Point: 205°C at 760 mmHg
• Flash Point: 79°C
• Density: 0.897g/cm³
• XLogP3: 1
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 4
• Exact Mass: 139.099714038
• Heavy Atom Count: 10
• Complexity: 130

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC(=O)N(CC=C)CC=C

Technology Process of N,N-bis(prop-2-en-1-yl)acetamide

There total 1 articles about N,N-bis(prop-2-en-1-yl)acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 37.0%

acetamide (60-35-5) + O-allyl-N,N'-dicyclohexyl isourea (92954-34-2) → N-allylacetamide (692-33-1) + N,N-diallylacetamide (6296-61-3)

Guidance literature:

With bis(dibenzylideneacetone)-palladium⁽⁰⁾; In N,N-dimethyl-formamide; at 60 ℃; for 2h;

DOI:10.1246/bcsj.58.2721

Reference yield: 96.0%

N,N-diallylacetamide (6296-61-3) + thiophenol (108-98-5) → 1-acetyl-3-methyl-4-(phenylsulfanylmethyl)-1-pyrrolidine

Guidance literature:

With α,α'-azodiizobutyramidine-dihydrochloride; In water; at 60 ℃; for 2h;

DOI:10.1016/S0040-4039(98)02391-0 DOI:10.1246/bcsj.74.1963

Reference yield: 85.0%

N,N-diallylacetamide (6296-61-3) + benzenediazonium tetrafluoroborate (369-57-3) → C20H21NO (692263-13-1)

Guidance literature:

With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; sodium acetate; In benzonitrile; at 20 ℃; regioselective reaction;

DOI:10.1016/j.tet.2013.10.014

upstream raw materials:

acetamide

O-allyl-N,N'-dicyclohexyl isourea

Downstream raw materials:

trans-N-acetyl-3-chloromethyl-4-(2,2,2-trichloroethyl)pyrrolidine

cis-N-acetyl-3-chloromethyl-4-(2,2,2-trichloroethyl)pyrrolidine

N-acetyl-3-bromomethyl-4-(2,2,2-trichloroethyl)pyrrolidine

N-(2-(5-bromo-1-((4-bromo-2-methoxyphenyl)amino)indol-3-yl)ethyl)acetamide