1-(3-chlorophenyl)-3-[(3-chlorophenyl)amino]-1H-pyrrole-2,5-dione

Base Information

• Chemical Name: 1-(3-chlorophenyl)-3-[(3-chlorophenyl)amino]-1H-pyrrole-2,5-dione
• CAS No.: 24978-27-6
• Molecular Formula: C16H10 Cl2 N2 O2
• Molecular Weight: 333.1688
• Mol file: 24978-27-6.mol

Synonyms:Maleimide,2-(m-chloroanilino)-N-(m-chlorophenyl)- (8CI); NSC 149812

Chemical Property of 1-(3-chlorophenyl)-3-[(3-chlorophenyl)amino]-1H-pyrrole-2,5-dione

Chemical Property:

• Vapor Pressure: 1.31E-09mmHg at 25°C
• Boiling Point: 486.3°C at 760 mmHg
• Flash Point: 247.9°C
• Density: 1.534g/cm³

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1-(3-chlorophenyl)-3-[(3-chlorophenyl)amino]-1H-pyrrole-2,5-dione

There total 3 articles about 1-(3-chlorophenyl)-3-[(3-chlorophenyl)amino]-1H-pyrrole-2,5-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(3-chloro-anilino)-butenedioic acid diethyl ester (97301-17-2) + 3-chloro-aniline (108-42-9) → 3-(3-chloro-anilino)-1-(3-chloro-phenyl)-pyrrole-2,5-dione (24978-27-6)

Guidance literature:

With acetic acid; at 180 - 190 ℃;

DOI:10.1021/ja01207a047

Reference yield:

3-chloro-aniline (108-42-9) → 3-(3-chloro-anilino)-1-(3-chloro-phenyl)-pyrrole-2,5-dione (24978-27-6)

Guidance literature:

Multi-step reaction with 2 steps

1: acetic acid

2: acetic acid / 180 - 190 °C

With acetic acid;

DOI:10.1021/ja01207a047

Reference yield:

→ 3-(3-chloro-anilino)-1-(3-chloro-phenyl)-pyrrole-2,5-dione (24978-27-6)

Guidance literature:

3-Chloranilin, Diethylacetylendicarboxylat;

upstream raw materials:

(3-chloro-anilino)-butenedioic acid diethyl ester

3-chloro-aniline