Imidazole-2-thiol, 1-butyl-

Base Information

Chemical Name:Imidazole-2-thiol, 1-butyl-
CAS No.:10583-85-4
Molecular Formula:C7H12 N2 S
Molecular Weight:156.252
Hs Code.:2933290090
DSSTox Substance ID:DTXSID50147358
Nikkaji Number:J86.871J
Mol file:10583-85-4.mol

Synonyms:Imidazole-2-thiol, 1-butyl-;USAF EL-64;10583-85-4;3-butyl-1H-imidazole-2-thione;1-n-Butyl-2-mercaptoimidazole;Imidazole, 1-n-butyl-2-mercapto-;1-Butyl-4-imidazoline-2-thione;SCHEMBL996895;DTXSID50147358;AKOS009271070;LS-78912

Suppliers and Price of Imidazole-2-thiol, 1-butyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
1-BUTYL-1H-IMIDAZOLE-2-THIOL 95.00%
5MG
$ 497.49

Total 5 raw suppliers

Chemical Property of Imidazole-2-thiol, 1-butyl-

Chemical Property:

Vapor Pressure:0.138mmHg at 25°C
Boiling Point:216.8°C at 760 mmHg
Flash Point:84.9°C
PSA：56.62000
Density:1.12g/cm³
LogP:1.97190
XLogP3:1.2
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:3
Exact Mass:156.07211956
Heavy Atom Count:10
Complexity:154

Purity/Quality:

98%,99%, ^*data from raw suppliers

1-BUTYL-1H-IMIDAZOLE-2-THIOL 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCCCN1C=CNC1=S

Technology Process of Imidazole-2-thiol, 1-butyl-

There total 5 articles about Imidazole-2-thiol, 1-butyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 162150-91-6
3-butyl-2-thioxoimidazolidin-4-one

: 10583-85-4
1-butylimidazole-2-thione

Guidance literature:: 3-butyl-2-thioxoimidazolidin-4-one; With sodium tetrahydroborate; lithium chloride; In 1,2-dimethoxyethane; ethanol; at -15 - -5 ℃; for 6h;

With hydrogenchloride; In 1,2-dimethoxyethane; ethanol; for 0.5h; Further stages.;
DOI:10.1055/s-2007-983740

Reference yield:

: 85694-91-3
n-butylaminoacetaldehyde diethyl acetale

: 333-20-0
potassium thioacyanate

: 10583-85-4
1-butylimidazole-2-thione

Guidance literature:: With hydrogenchloride; ethanol;
DOI:10.1021/ja01180a036

Reference yield:

: 92503-17-8
5-butyl-4-thio-hydantoic acid

: 10583-85-4
1-butylimidazole-2-thione

Guidance literature:: Multi-step reaction with 2 steps

1.1: 7.49 g / aq. H₂SO₄ / acetone

2.1: NaBH₄; LiCl / 1,2-dimethoxy-ethane; ethanol / 6 h / -15 - -5 °C

2.2: 97 percent / conc. HCl / 1,2-dimethoxy-ethane; ethanol / 0.5 h

With sodium tetrahydroborate; sulfuric acid; lithium chloride; In 1,2-dimethoxyethane; ethanol; acetone;
DOI:10.1055/s-2007-983740