(8)-Gingerdione

Base Information

Chemical Name:(8)-Gingerdione
CAS No.:77334-06-6
Deprecated CAS:1339934-25-6
Molecular Formula:C₁₉H₂₈O₄
Molecular Weight:320.429
Hs Code.:
UNII:70E1Y63Q2L
DSSTox Substance ID:DTXSID801316888
Nikkaji Number:J1.730.479H
Wikidata:Q27265857

Synonyms:(8)-Gingerdione;8-Gingerdione;77334-06-6;[8]-Gingerdione;UNII-70E1Y63Q2L;70E1Y63Q2L;3,5-Dodecanedione, 1-(4-hydroxy-3-methoxyphenyl)-;1-(4-Hydroxy-3-methoxyphenyl)dodecane-3,5-dione;4-Dodecen-3-one, 5-hydroxy-1-(4-hydroxy-3-methoxyphenyl)-, (4Z)-;CHEBI:175095;QDSRAFNZQKMHPZ-UHFFFAOYSA-N;DTXSID801316888;3-(octadecylcarbamoyl)-2-sulfo-propanoic Acid;8-GINGERDIONE: N=6 (CONSTITUENT OF GINGER);Q27265857;1-(4-Hydroxy-3-methoxyphenyl)-3,5-dodecanedione, 9CI;8-GINGERDIONE : N=6 (CONSTITUENT OF GINGER) [DSC]

Suppliers and Price of (8)-Gingerdione

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of (8)-Gingerdione

Chemical Property:

XLogP3:3.7
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:12
Exact Mass:320.19875937
Heavy Atom Count:23
Complexity:353

Purity/Quality:: > 95% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCCCCCCC(=O)CC(=O)CCC1=CC(=C(C=C1)O)OC

Technology Process of (8)-Gingerdione

There total 4 articles about (8)-Gingerdione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1080-12-2,22214-42-2
(E)-4-(4-hydroxy-3-methoxyphenyl)but-3-ene-2-one

: 77334-06-6
<8>-gingerdione

Guidance literature:: Multi-step reaction with 3 steps

1: 86 percent / H₂ / Raney nickel / acetone

2: 84 percent / phenol, hexamethyldisilazane / benzene / Heating

3: 1.) lithium bis(trimethylsilyl)amide, 2.) hydrochloric acid / 1.) THF, -78 deg C, 1.5 h, 2.) water

With hydrogenchloride; hydrogen; 1,1,1,3,3,3-hexamethyl-disilazane; lithium hexamethyldisilazane; phenol; nickel; In acetone; benzene;
DOI:10.1039/P19810000082

Reference yield:

: 121-33-5,8014-42-4
vanillin

: 77334-06-6
<8>-gingerdione

Guidance literature:: Multi-step reaction with 4 steps

1: 82 percent / 10percent aq. sodium hydroxide / 96 h

2: 86 percent / H₂ / Raney nickel / acetone

3: 84 percent / phenol, hexamethyldisilazane / benzene / Heating

4: 1.) lithium bis(trimethylsilyl)amide, 2.) hydrochloric acid / 1.) THF, -78 deg C, 1.5 h, 2.) water

With hydrogenchloride; sodium hydroxide; hydrogen; 1,1,1,3,3,3-hexamethyl-disilazane; lithium hexamethyldisilazane; phenol; nickel; In acetone; benzene;
DOI:10.1039/P19810000082

Reference yield:

: 122-48-5
4-(4-hydroxy-3-methoxyphenyl)-2-butanone

: 77334-06-6
<8>-gingerdione

Guidance literature:: Multi-step reaction with 2 steps

1: 84 percent / phenol, hexamethyldisilazane / benzene / Heating

2: 1.) lithium bis(trimethylsilyl)amide, 2.) hydrochloric acid / 1.) THF, -78 deg C, 1.5 h, 2.) water

With hydrogenchloride; 1,1,1,3,3,3-hexamethyl-disilazane; lithium hexamethyldisilazane; phenol; In benzene;
DOI:10.1039/P19810000082