Squalene N-methylimine

Base Information

• Chemical Name: Squalene N-methylimine
• CAS No.: 123453-64-5
• Molecular Formula: C₂₈H₄₇N
• Molecular Weight: 397.688
• Mol file: 123453-64-5.mol

Synonyms:squalene N-methylimine

Chemical Property of Squalene N-methylimine

Chemical Property:

• Vapor Pressure: 7.63E-10mmHg at 25°C
• Boiling Point: 505.5°Cat760mmHg
• Flash Point: 252.6°C
• PSA: 12.36000
• Density: 0.82g/cm³
• LogP: 9.33940
• XLogP3: 9.2
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 15
• Exact Mass: 397.370850503
• Heavy Atom Count: 29
• Complexity: 604

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC(=CCCC(=CCCC(=CCCC=C(C)CCC=C(C)CCC=NC)C)C)C
• Isomeric SMILES: CC(=CCC/C(=C/CC/C(=C/CC/C=C(\C)/CC/C=C(\C)/CCC=NC)/C)/C)C

Technology Process of Squalene N-methylimine

There total 1 articles about Squalene N-methylimine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(4E,8E,12E,16E)-4,8,13,17,21-pentamethyldocosa-4,8,12,16,20-pentaenal (56882-05-4) + methylamine (74-89-5) → (4E,8E,12E,16E)-N-(4,8,13,17,21-pentamethyl-4,8,12,16,20-docosapentaenylidne)methylamine (123453-64-5)

Guidance literature:

With potassium hydroxide; Yield given; 1.) -10 deg C, 45 min; 2.) -10 deg C, 15 min, then up to RT;

DOI:10.1016/0223-5234(88)90096-7

Reference yield:

(4E,8E,12E,16E)-N-(4,8,13,17,21-pentamethyl-4,8,12,16,20-docosapentaenylidne)methylamine (123453-64-5) → (3E,7E,11E,15E)-2-methyl-3-(3,7,12,16,20-pentamethyl-3,7,11,15,19-henicosapentaenyl)oxaziridine (126267-95-6)

Guidance literature:

With sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; for 1h; Yield given;

DOI:10.1016/0223-5234(88)90096-7

upstream raw materials:

(4E,8E,12E,16E)-4,8,13,17,21-pentamethyldocosa-4,8,12,16,20-pentaenal

methylamine

Downstream raw materials:

(3E,7E,11E,15E)-2-methyl-3-(3,7,12,16,20-pentamethyl-3,7,11,15,19-henicosapentaenyl)oxaziridine