Arsine, chloroethyl(4-methoxyphenyl)-

Base Information

• Chemical Name: Arsine, chloroethyl(4-methoxyphenyl)-
• CAS No.: 61130-95-8
• Molecular Formula: C9H12AsClO
• Molecular Weight: 246.568
• DSSTox Substance ID: DTXSID50210016
• Wikidata: Q83084541
• Mol file: 61130-95-8.mol

Synonyms:Ethyl-p-anisylchloroarsine;Arsine, chloroethyl(4-methoxyphenyl)-;BRN 2937339;Chloroethyl(p-methoxyphenyl)arsine;61130-95-8;C9H12AsClO;C9-H12-As-Cl-O;DTXSID50210016;LS-21809

Chemical Property of Arsine, chloroethyl(4-methoxyphenyl)-

Chemical Property:

• Vapor Pressure: 0.00262mmHg at 25°C
• Boiling Point: 295.9°C at 760 mmHg
• Flash Point: 96.2°C
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 3
• Exact Mass: 245.979262
• Heavy Atom Count: 12
• Complexity: 124

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: CC[As](C1=CC=C(C=C1)OC)Cl

Technology Process of Arsine, chloroethyl(4-methoxyphenyl)-

There total 2 articles about Arsine, chloroethyl(4-methoxyphenyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

p-anisylarsine dichloride (65452-83-7) + tetraethyllead(IV) (78-00-2) → chloroethane (75-00-3) + chloroethyl(p-methoxyphenyl)arsine (61130-95-8)

Guidance literature:

at 90 - 110 ℃;

Reference yield:

→ chloroethyl(p-methoxyphenyl)arsine (61130-95-8)

Guidance literature:

entspr. Dichlorarsin, Et4Pb;

Reference yield: 82.0%

chloroethyl(p-methoxyphenyl)arsine (61130-95-8) + tert-butylamine (75-64-9) → N-tert-butylamido(ethyl)-p-anisylarsinite (139455-53-1)

Guidance literature:

In benzene; for 2h;

upstream raw materials:

p-anisylarsine dichloride

tetraethyllead(IV)

Downstream raw materials:

N-tert-butylamido(ethyl)-p-anisylarsinite