Bis(2-azanidylethyl)azanide; trichlorocobalt

Base Information

Chemical Name:Bis(2-azanidylethyl)azanide; trichlorocobalt
CAS No.:15025-06-6
Molecular Formula:C₄H₁₃Cl₃CoN₃
Molecular Weight:268.52
Hs Code.:
Mol file:15025-06-6.mol

Synonyms:

Suppliers and Price of Bis(2-azanidylethyl)azanide; trichlorocobalt

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 7 raw suppliers

Chemical Property of Bis(2-azanidylethyl)azanide; trichlorocobalt

Chemical Property:

Boiling Point:206.9 °C at 760 mmHg
Flash Point:94.4 °C

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of Bis(2-azanidylethyl)azanide; trichlorocobalt

There total 4 articles about Bis(2-azanidylethyl)azanide; trichlorocobalt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: trinitro(diethylenetriamine)cobalt(III)

: 92273-55-7,15025-06-6,131903-58-7,14215-59-9
(3-azapentane-1,5-diamine)trichlorocobalt(III)

Guidance literature:: With HCl; In hydrogenchloride; byproducts: NO2; heating of Co-complex with concd. HCl; pptn. on cooling, washing (Me2CO); elem. anal.;
DOI:10.1039/DT9770001215

Reference yield:

: trinitro(diethylenetriamine)cobalt(III)

: 131903-58-7,14215-59-9,15025-06-6,92273-55-7
mer-{(3-azapentane-1,5-diamine)trichlorocobalt(III)}

Guidance literature:: With hydrogenchloride; In hydrogenchloride; 80-90°C, 3 h; washing (2-propanol, ether), drying in air;
DOI:10.1016/S0020-1693(00)91593-7

Reference yield:

: trinitro(diethylenetriamine)cobalt(III)

: 131903-58-7,14215-59-9,15025-06-6,92273-55-7
mer-{(3-azapentane-1,5-diamine)trichlorocobalt(III)}

: chlorodinitro(diethylenetriamine)cobalt(III)

Guidance literature:: With hydrogenchloride; In hydrogenchloride; byproducts: NO2; suspn. of Co-complex in 12 M HCl, heating (350 -360 K, 3 ks); collection, recrystn. (from aq. NaOH by 12 M HCl; cooling), collection; IR spectroscopy;
DOI:10.1016/S0020-1693(00)89488-8