3-(prop-2-en-1-yl)-1,2,3-benzotriazin-4(3H)-one

Base Information

Chemical Name:3-(prop-2-en-1-yl)-1,2,3-benzotriazin-4(3H)-one
CAS No.:25465-49-0
Molecular Formula:C₁₀H₉N₃O
Molecular Weight:187.201
Hs Code.:
Mol file:25465-49-0.mol

Synonyms:1,2,3-Benzotriazin-4(3H)-one,3-(2-propenyl)- (9CI); 1,2,3-Benzotriazin-4(3H)-one, 3-allyl- (8CI); NSC 279261

Suppliers and Price of 3-(prop-2-en-1-yl)-1,2,3-benzotriazin-4(3H)-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of 3-(prop-2-en-1-yl)-1,2,3-benzotriazin-4(3H)-one

Chemical Property:

Vapor Pressure:0.000744mmHg at 25°C
Boiling Point:307°C at 760 mmHg
Flash Point:139.5°C
Density:1.22g/cm³

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 3-(prop-2-en-1-yl)-1,2,3-benzotriazin-4(3H)-one

There total 5 articles about 3-(prop-2-en-1-yl)-1,2,3-benzotriazin-4(3H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 90-16-4
1,2,3-benzotriazin-4(3H)-one

: 106-95-6
allyl bromide

: 25465-49-0
N³-allylbenzotriazinone

Guidance literature:: With potassium carbonate; In acetone; for 14h; Schlenk technique; Reflux;
DOI:10.1021/acs.orglett.0c00397

Reference yield: 79.0%

: 90-16-4
1,2,3-benzotriazin-4(3H)-one

: 107-18-6
allyl alcohol

: 25465-49-0
N³-allylbenzotriazinone

Guidance literature:: With triphenylphosphine; diethylazodicarboxylate; In 1,4-dioxane; for 2h; Ambient temperature;
DOI:10.1021/jo00125a009

Reference yield:

: 3-(2-phenylpropan-2-yl)benzo[d][1,2,3]triazin-4(3H)-one

: 25465-49-0
N³-allylbenzotriazinone

Guidance literature:: Multi-step reaction with 2 steps

1: trifluoroacetic acid / 0 - 20 °C

2: potassium carbonate / acetone / 14 h / Schlenk technique; Reflux

With potassium carbonate; trifluoroacetic acid; In acetone;
DOI:10.1021/acs.orglett.0c00397