3-(2,3-dimethoxyphenyl)propyl phenylcarbamate

Base Information

• Chemical Name: 3-(2,3-dimethoxyphenyl)propyl phenylcarbamate
• CAS No.: 7461-68-9
• Molecular Formula: C₁₈H₂₁NO₄
• Molecular Weight: 315.369
• Mol file: 7461-68-9.mol

Synonyms:Benzenepropanol,2,3-dimethoxy-, phenylcarbamate (9CI); NSC 403624

Chemical Property of 3-(2,3-dimethoxyphenyl)propyl phenylcarbamate

Chemical Property:

• Vapor Pressure: 4.25E-07mmHg at 25°C
• Boiling Point: 415°Cat760mmHg
• Flash Point: 204.8°C
• Density: 1.165g/cm³

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3-(2,3-dimethoxyphenyl)propyl phenylcarbamate

There total 3 articles about 3-(2,3-dimethoxyphenyl)propyl phenylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(E)-ethyl 3-(2,3-dimethoxyphenyl)prop-2-enoate (79618-90-9) → 1-(2,3-dimethoxy-phenyl)-3-phenylcarbamoyloxy-propane (7461-68-9)

Guidance literature:

Multi-step reaction with 2 steps

1: copper oxide-chromium oxide / 225 °C / 139746 Torr / Hydrogenation

With copper oxide-chromium oxide;

DOI:10.1021/ja01201a514

Reference yield:

2,3-dimethyoxybenzaldehyde (86-51-1) → 1-(2,3-dimethoxy-phenyl)-3-phenylcarbamoyloxy-propane (7461-68-9)

Guidance literature:

Multi-step reaction with 3 steps

1: sodium; ethyl acetate; ethanol

2: copper oxide-chromium oxide / 225 °C / 139746 Torr / Hydrogenation

With ethanol; copper oxide-chromium oxide; sodium; ethyl acetate;

DOI:10.1021/ja01201a514

Reference yield:

3-(2,3-dimethoxyphenyl)propan-1-ol (103853-10-7) + phenyl isocyanate (103-71-9) → 1-(2,3-dimethoxy-phenyl)-3-phenylcarbamoyloxy-propane (7461-68-9)

Guidance literature:

DOI:10.1021/ja01201a514

upstream raw materials:

3-(2,3-dimethoxyphenyl)propan-1-ol

phenyl isocyanate

(E)-ethyl 3-(2,3-dimethoxyphenyl)prop-2-enoate

2,3-dimethyoxybenzaldehyde