Mesaconine

Base Information

• Chemical Name: Mesaconine
• CAS No.: 6792-09-2
• Molecular Formula: C24H39NO9
• Molecular Weight: 485.57

Synonyms:(15S,16S)-1α,6α,16-Trimethoxy-4-methoxymethyl-20-methyl-aconitan-3α,8,13,14α,15-pentaol;(15S,16S)-1α,6α,16-trimethoxy-4-methoxymethyl-20-methyl-aconitane-3α,8,13,14α,15-pentaol;mesaconine;

Chemical Property of Mesaconine

Chemical Property:

• Boiling Point: 617.1±55.0 °C(Predicted)
• PKA: 12.22±0.70(Predicted)
• PSA: 141.31000
• Density: 1.44±0.1 g/cm3(Predicted)
• LogP: -2.23960

Purity/Quality:

99%, ^*data from raw suppliers

Mesaconine ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Mesaconine

There total 5 articles about Mesaconine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.1%

3,14,15-triacetylmesaconine → Mesaconine (6792-09-2)

Guidance literature:

With ethanol; sodium hydroxide; for 0.5h; Reflux;

Reference yield:

Aconine (509-20-6) → Mesaconine (6792-09-2)

Guidance literature:

Multi-step reaction with 4 steps

1.1: pyridine / 2.5 h / Reflux

2.1: N-Bromosuccinimide; acetic acid / 2 h / 20 °C

3.1: acetic acid / water; tetrahydrofuran / 0.5 h / 20 °C

3.2: 0.5 h

4.1: sodium hydroxide; ethanol / 0.5 h / Reflux

With pyridine; N-Bromosuccinimide; ethanol; acetic acid; sodium hydroxide; In tetrahydrofuran; water;

Reference yield:

3,14,15-triacetylaconine → Mesaconine (6792-09-2)

Guidance literature:

Multi-step reaction with 3 steps

1.1: N-Bromosuccinimide; acetic acid / 2 h / 20 °C

2.1: acetic acid / water; tetrahydrofuran / 0.5 h / 20 °C

2.2: 0.5 h

3.1: sodium hydroxide; ethanol / 0.5 h / Reflux

With N-Bromosuccinimide; ethanol; acetic acid; sodium hydroxide; In tetrahydrofuran; water;

upstream raw materials:

Aconine

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