(1H-Benzotriazol-1-yl)-N,N,N-trimethylmethanaminium iodide

Base Information

Chemical Name:(1H-Benzotriazol-1-yl)-N,N,N-trimethylmethanaminium iodide
CAS No.:57684-34-1
Molecular Formula:C10H15N4+
Molecular Weight:191.2524
Hs Code.:
DSSTox Substance ID:DTXSID10562503
NSC Number:130835

Synonyms:57684-34-1;DTXSID10562503;(1H-Benzotriazol-1-yl)-N,N,N-trimethylmethanaminium iodide;NSC130835;NSC-130835

Suppliers and Price of (1H-Benzotriazol-1-yl)-N,N,N-trimethylmethanaminium iodide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of (1H-Benzotriazol-1-yl)-N,N,N-trimethylmethanaminium iodide

Chemical Property:

Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:2
Exact Mass:318.03414
Heavy Atom Count:15
Complexity:199

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C[N+](C)(C)CN1C2=CC=CC=C2N=N1.[I-]

Technology Process of (1H-Benzotriazol-1-yl)-N,N,N-trimethylmethanaminium iodide

There total 4 articles about (1H-Benzotriazol-1-yl)-N,N,N-trimethylmethanaminium iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 54187-96-1
1-(chloromethyl)-1H-benzotriazole

: 75-50-3
trimethylamine

: 57684-34-1
1-(1H-benzo[d][1,2,3]triazol-1-yl)-N,N,N-trimethylmethanaminium iodide

Guidance literature:: 1-(chloromethyl)-1H-benzotriazole; With potassium iodide; In acetone; for 2h;

trimethylamine; In acetone; at 20 ℃;
DOI:10.1021/jacs.7b04550

Reference yield:

: 54187-96-1
1-(chloromethyl)-1H-benzotriazole

: 57684-34-1
1-(1H-benzo[d][1,2,3]triazol-1-yl)-N,N,N-trimethylmethanaminium iodide

Guidance literature:: Multi-step reaction with 2 steps

1: NaI / acetone / 4 h / Ambient temperature

With sodium iodide; In acetone;

Reference yield:

: 95-14-7,27556-51-0
1,2,3-Benzotriazole

: 57684-34-1
1-(1H-benzo[d][1,2,3]triazol-1-yl)-N,N,N-trimethylmethanaminium iodide

Guidance literature:: Multi-step reaction with 3 steps

1.1: water / 1.5 h / Reflux

2.1: thionyl chloride / N,N-dimethyl-formamide; dichloromethane / 2 h / 20 °C

3.1: potassium iodide / acetone / 2 h

3.2: 20 °C

With thionyl chloride; potassium iodide; In dichloromethane; water; N,N-dimethyl-formamide; acetone; 1.1: |Menshutkin Reaction / 3.2: |Menshutkin Reaction;
DOI:10.1021/jacs.7b04550