2-chloro-6-[(methylsulfanyl)methyl]aniline

Base Information

Chemical Name:2-chloro-6-[(methylsulfanyl)methyl]aniline
CAS No.:34774-88-4
Molecular Formula:C8H10 Cl N S
Molecular Weight:187.693
Hs Code.:
Mol file:34774-88-4.mol

Synonyms:2-Chloro-6-(methylthiomethyl)aniline;NSC 298394; [2-Chloro-6-[(methylsulfanyl)methyl]phenyl]amine

Suppliers and Price of 2-chloro-6-[(methylsulfanyl)methyl]aniline

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of 2-chloro-6-[(methylsulfanyl)methyl]aniline

Chemical Property:

Vapor Pressure:0.00235mmHg at 25°C
Boiling Point:288.3°Cat760mmHg
Flash Point:128.2°C
Density:1.247g/cm³

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2-chloro-6-[(methylsulfanyl)methyl]aniline

There total 5 articles about 2-chloro-6-[(methylsulfanyl)methyl]aniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 41.0%

: 75-18-3
dimethylsulfide

: 3296-07-9
1-azido-2-chlorobenzene

: 624-92-0
Dimethyldisulphide

: 34774-88-4
6-Chloro-(α-methylthio)-o-toluidine

: 95-51-2
o-chloroaniline

Guidance literature:: at 155 ℃; for 10h; Yields of byproduct given;

Reference yield:

: 20094-93-3
N-(2-chlorophenyl)-S,S-dimethylsulfilimine

: 34774-88-4
6-Chloro-(α-methylthio)-o-toluidine

Guidance literature:: With sodium methylate; In methanol; dichloromethane; acetonitrile; at -78 - 20 ℃; for 12h; Inert atmosphere;
DOI:10.1002/adsc.201600823

Reference yield:

: 95-51-2
o-chloroaniline

: 34774-88-4
6-Chloro-(α-methylthio)-o-toluidine

Guidance literature:: Multi-step reaction with 2 steps

1: trifluoroacetic anhydride / acetonitrile; dichloromethane / 5 h / -78 °C / Inert atmosphere

2: sodium methylate / acetonitrile; dichloromethane; methanol / 12 h / -78 - 20 °C / Inert atmosphere

With sodium methylate; trifluoroacetic anhydride; In methanol; dichloromethane; acetonitrile;
DOI:10.1002/adsc.201600823