Butyloxycarbonyl-cholecystokinin (31-33) amide

Base Information

Chemical Name:Butyloxycarbonyl-cholecystokinin (31-33) amide
CAS No.:5920-14-9
Molecular Formula:C23H34 N4 O7 S
Molecular Weight:510.612
Hs Code.:
DSSTox Substance ID:DTXSID50974626
Mol file:5920-14-9.mol

Synonyms:Boc-CCK (31-33)-NH2;butyloxycarbonyl-cholecystokinin (31-33) amide;cholecystokinin (31-33) amide, butyloxycarbonyl-;cholecystokinin (31-33)-NH2, butyloxycarbonyl-

Suppliers and Price of Butyloxycarbonyl-cholecystokinin (31-33) amide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
BOC-MET-ASP-PHE AMIDE 95.00%
5MG
$ 502.10

Total 4 raw suppliers

Chemical Property of Butyloxycarbonyl-cholecystokinin (31-33) amide

Chemical Property:

Vapor Pressure:5.93E-32mmHg at 25°C
Boiling Point:865.3°C at 760 mmHg
Flash Point:477.1°C
PSA：213.68000
Density:1.262g/cm³
LogP:3.83980
Storage Temp.:−20°C
XLogP3:1.1
Hydrogen Bond Donor Count:5
Hydrogen Bond Acceptor Count:8
Rotatable Bond Count:15
Exact Mass:510.21482061
Heavy Atom Count:35
Complexity:751

Purity/Quality:

97% ^*data from raw suppliers

BOC-MET-ASP-PHE AMIDE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(C)(C)OC(=O)NC(CCSC)C(=O)NC(CC(=O)O)C(=O)NC(CC1=CC=CC=C1)C(=O)N
Isomeric SMILES:CC(C)(C)OC(=O)N[C@@H](CCSC)C(=O)N[C@@H](CC(=O)O)C(=O)N[C@@H](CC1=CC=CC=C1)C(=O)N

Technology Process of Butyloxycarbonyl-cholecystokinin (31-33) amide

There total 6 articles about Butyloxycarbonyl-cholecystokinin (31-33) amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 5241-71-4
Asp-Phe-NH₂

: 16948-13-3
Boc-Met-OTcp

: 5920-14-9
N^α-tert-Butyloxycarbonyl-L-methionyl-L-aspartyl-L-phenylalanine amide

Guidance literature:: With 4-methyl-morpholine; In N,N-dimethyl-formamide; for 40h; Ambient temperature;
DOI:10.1248/cpb.36.3915

Reference yield:

: 5241-68-9
Z-Asp(OBzl)-Phe-NH₂

: 5920-14-9
N^α-tert-Butyloxycarbonyl-L-methionyl-L-aspartyl-L-phenylalanine amide

Guidance literature:: Multi-step reaction with 2 steps

1: 83 percent / H₂ / Pd / dimethylformamide; H₂O

2: 85 percent / N-methylmorpholine / dimethylformamide / 40 h / Ambient temperature

With 4-methyl-morpholine; hydrogen; palladium; In water; N,N-dimethyl-formamide;
DOI:10.1248/cpb.36.3915

Reference yield:

: 65864-22-4
(S)-2-amino-3-phenylpropionamide hydrochloride

: 5920-14-9
N^α-tert-Butyloxycarbonyl-L-methionyl-L-aspartyl-L-phenylalanine amide

Guidance literature:: Multi-step reaction with 3 steps

1: 85 percent / Et₃N / dimethylformamide / 16 h

2: 83 percent / H₂ / Pd / dimethylformamide; H₂O

3: 85 percent / N-methylmorpholine / dimethylformamide / 40 h / Ambient temperature

With 4-methyl-morpholine; hydrogen; triethylamine; palladium; In water; N,N-dimethyl-formamide;
DOI:10.1248/cpb.36.3915