1-Oxo-1H-pyrimido[1,2-a]quinoline-2-carboxylic acid ethyl ester

Base Information

Chemical Name:1-Oxo-1H-pyrimido[1,2-a]quinoline-2-carboxylic acid ethyl ester
CAS No.:37611-65-7
Molecular Formula:C15H12N2O3
Molecular Weight:0
Hs Code.:
Mol file:37611-65-7.mol

Synonyms:1-Oxo-1H-pyrido<1,2-a>chinolin-2-carbonsaeure-ethylester;2-Ethoxycarbonyl-1-oxo-1H-pyrimido<1,2-a>quinoline;

Suppliers and Price of 1-Oxo-1H-pyrimido[1,2-a]quinoline-2-carboxylic acid ethyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of 1-Oxo-1H-pyrimido[1,2-a]quinoline-2-carboxylic acid ethyl ester

Chemical Property:

Vapor Pressure:4.34E-07mmHg at 25°C
Boiling Point:414.8°C at 760 mmHg
Flash Point:204.6°C
PSA：60.67000
Density:1.31g/cm³
LogP:2.02440

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 1-Oxo-1H-pyrimido[1,2-a]quinoline-2-carboxylic acid ethyl ester

There total 7 articles about 1-Oxo-1H-pyrimido[1,2-a]quinoline-2-carboxylic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 40519-79-7
diethyl 2-((quinolin-2-ylamino)methylene)malonate

: 37611-65-7
2-Ethoxycarbonyl-1-oxo-1H-pyrimido<1,2-a>quinoline

Guidance literature:: In tetrahydrofuran; at 390 ℃; under 75007.5 Torr;
DOI:10.1021/acs.joc.6b02520

Reference yield:

: 580-17-6
3-aminoquinoline

: 87-13-8
diethyl 2-ethoxymethylenemalonate

: 37611-65-7
2-Ethoxycarbonyl-1-oxo-1H-pyrimido<1,2-a>quinoline

Guidance literature:: With diphenylether; biphenyl;
DOI:10.1021/jo01152a016

Reference yield:

: O,O-Diethyl N-(2-quinolinyl)-aminomethylenethiomalonate

: 37611-65-7
2-Ethoxycarbonyl-1-oxo-1H-pyrimido<1,2-a>quinoline

Guidance literature:: With PPA; sodium hydrogencarbonate; trichlorophosphate; Yield given. Multistep reaction; 1.) 140 deg C, 5 h; 2.) room temp., pH 7;
DOI:10.1055/s-1984-30763