n,n,3-Trimethyl-4-nitrosoaniline

Base Information

• Chemical Name: n,n,3-Trimethyl-4-nitrosoaniline
• CAS No.: 29785-93-1
• Molecular Formula: C9H12 N2 O
• Molecular Weight: 164.207
• NSC Number: 37563
• DSSTox Substance ID: DTXSID10952223
• Nikkaji Number: J673.245C
• Wikidata: Q82930753
• Mol file: 29785-93-1.mol

Synonyms:n,n,3-trimethyl-4-nitrosoaniline;29785-93-1;NSC37563;SCHEMBL145777;DTXSID10952223;NSC-37563

Chemical Property of n,n,3-Trimethyl-4-nitrosoaniline

Chemical Property:

• Vapor Pressure: 0.0026mmHg at 25°C
• Boiling Point: 286.7°C at 760 mmHg
• Flash Point: 127.2°C
• Density: 1.03g/cm³
• XLogP3: 1.8
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 1
• Exact Mass: 164.094963011
• Heavy Atom Count: 12
• Complexity: 159

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC1=C(C=CC(=C1)N(C)C)N=O

Technology Process of n,n,3-Trimethyl-4-nitrosoaniline

There total 5 articles about n,n,3-Trimethyl-4-nitrosoaniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

chloro(cyclo-octa-1,5-diene){4-dimethylamino-2-methyl(nitroso)benzene-N'}rhodium(I) → di-μ-chloro-bis(1,5-cyclooctadiene)dirhodium (12092-47-6) + 4-dimethylamino-2-methyl(nitroso)benzene (29785-93-1)

Guidance literature:

In chloroform-d1; partial dissociation on increasing temp.; NMR; Kinetics;

Reference yield:

N,N-dimethyl-m-toluidine (121-72-2) → 4-dimethylamino-2-methyl(nitroso)benzene (29785-93-1)

Guidance literature:

With hydrogenchloride; water; sodium nitrite; anschliessend mit Soda;

Reference yield:

N,N-dimethyl-m-toluidine (121-72-2) + tetranitromethane (509-14-8) → 4-dimethylamino-2-methyl(nitroso)benzene (29785-93-1)

Guidance literature:

With hydrogenchloride;

upstream raw materials:

N,N-dimethyl-m-toluidine

tetranitromethane

hydrogenchloride

Downstream raw materials:

3-methyl-4-nitroso-phenol

2,N,N'-trimethyl-p-phenylenediamine

cyano-(4-dimethylamino-2-methyl-phenylimino)-acetic acid methyl ester

5-(dimethylamino)-2-nitrotoluene