8-phenyl-1,5,7,9-tetrazabicyclo[4.3.0]nona-2,4,6,8-tetraene

Base Information

Chemical Name:8-phenyl-1,5,7,9-tetrazabicyclo[4.3.0]nona-2,4,6,8-tetraene
CAS No.:55643-77-1
Molecular Formula:C11H8N4
Molecular Weight:196.211
Hs Code.:
Mol file:55643-77-1.mol

Synonyms:2-Phenyl-1,2,4-triazolo<2,3-a>pyrimidin;2-Phenyl-s-triazolo<1,5-a>pyrimidin;8-PHENYL-1,5,7,9-TETRAZABICYCLO[4.3.0]NONA-2,4,6,8-TETRAENE;2-phenyl<1,2,4>triazolo<1,5-a>pyrimidine;

Suppliers and Price of 8-phenyl-1,5,7,9-tetrazabicyclo[4.3.0]nona-2,4,6,8-tetraene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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Total 5 raw suppliers

Chemical Property of 8-phenyl-1,5,7,9-tetrazabicyclo[4.3.0]nona-2,4,6,8-tetraene

Chemical Property:

PSA：43.08000
Density:1.31g/cm³
LogP:1.79130

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 8-phenyl-1,5,7,9-tetrazabicyclo[4.3.0]nona-2,4,6,8-tetraene

There total 8 articles about 8-phenyl-1,5,7,9-tetrazabicyclo[4.3.0]nona-2,4,6,8-tetraene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 99806-14-1
N-(pyrimidin-2-yl)benzimidamide

: 55643-77-1
2-phenyl<1,2,4>triazolo<1,5-a>pyrimidine

Guidance literature:: With iodine; potassium carbonate; potassium iodide; In dimethyl sulfoxide; at 20 - 100 ℃;
DOI:10.1021/acs.joc.5b01183

Reference yield: 77.0%

: 4922-98-9
5-phenyl-1H-1,2,4-triazol-3-amine

: 102-52-3
malonaldehydebis(dimethylacetal)

: 55643-77-1
2-phenyl<1,2,4>triazolo<1,5-a>pyrimidine

Guidance literature:: With acetic acid; In water; for 4h; Reflux;
DOI:10.24820/ARK.5550190.P011.247

Reference yield: 71.0%

: 274-98-6
[1,2,4]triazolo[4,3-a]pyrimidine

: 591-50-4
iodobenzene

: 55643-77-1
2-phenyl<1,2,4>triazolo<1,5-a>pyrimidine

Guidance literature:: [1,2,4]triazolo[4,3-a]pyrimidine; iodobenzene; With copper(l) iodide; potassium carbonate; triphenylphosphine; Trimethylacetic acid; In 1,4-dioxane; dimethyl sulfoxide; at 120 ℃; for 24h; Inert atmosphere; Schlenk technique;

With formic acid; In 1,4-dioxane; dimethyl sulfoxide; at 110 ℃; for 12h; Reagent/catalyst; Solvent; Temperature; regioselective reaction; Catalytic behavior; Mechanism;
DOI:10.1021/jacs.6b03890