6-chloro-2-methylquinoxaline

Base Information

Chemical Name:6-chloro-2-methylquinoxaline
CAS No.:1932-67-8
Molecular Formula:C9H7ClN2
Molecular Weight:178.6183
Hs Code.:

Synonyms:

Suppliers and Price of 6-chloro-2-methylquinoxaline

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 8 raw suppliers

Chemical Property of 6-chloro-2-methylquinoxaline

Chemical Property:

Vapor Pressure:0.00605mmHg at 25°C
Boiling Point:281.5°C at 760 mmHg
Flash Point:151°C
Density:1.292g/cm³

Purity/Quality:: 97% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 6-chloro-2-methylquinoxaline

There total 8 articles about 6-chloro-2-methylquinoxaline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 18671-97-1
2,6-dichloroquinoxaline

: 75-16-1
methylmagnesium bromide

: 1932-67-8
6-chloro-2-methylquinoxaline

Guidance literature:: With 1-methyl-pyrrolidin-2-one; iron(II) acetylacetonate; In tetrahydrofuran; toluene; at 20 ℃;
DOI:10.1002/adsc.200900522

Reference yield:

: 95-83-0
4-Chloro-1,2-phenylenediamine

: 78-98-8
2-oxopropanal

: 1831-88-5
7-chloro-2-methylquinoxaline

: 1932-67-8
6-chloro-2-methylquinoxaline

Guidance literature:: In water; at 20 ℃; for 0.5h; Overall yield = >95 %; Green chemistry;
DOI:10.1055/s-0033-1338441

Reference yield:

: 89284-67-3
1-azido-4-methyl-2-nitrobenzene

: 1932-67-8
6-chloro-2-methylquinoxaline

Guidance literature:: Multi-step reaction with 3 steps

1: 92 percent / benzene / Ambient temperature

2: NaBH₄ / Cu(II) acetylacetonate / ethanol; propan-2-ol / 6 h / 30 °C

3: 2) 2,3-dichloro-5,6-dicyanobenzoquinone / 1) toluene, reflux, 1 h, 2) THF, RT, 3-6 h

With sodium tetrahydroborate; 2,3-dicyano-5,6-dichloro-p-benzoquinone; copper acetylacetonate; In ethanol; isopropyl alcohol; benzene;