5-ALLYLSULFANYL-[1,3,4]THIADIAZOL-2-YLAMINE

Base Information

• Chemical Name: 5-ALLYLSULFANYL-[1,3,4]THIADIAZOL-2-YLAMINE
• CAS No.: 30062-44-3
• Molecular Formula: C5H7 N3 S2
• Molecular Weight: 173.263
• Hs Code.: 2934999090
• Mol file: 30062-44-3.mol

Synonyms:1,3,4-Thiadiazol-2-amine,5-(2-propenylthio)- (9CI); 1,3,4-Thiadiazole, 2-(allylthio)-5-amino- (7CI);2-Amino-5-allylthio-1,2,4-thiadiazol; 2-Amino-5-allylthio-1,3,4-thiadiazole;NSC 523975

Chemical Property of 5-ALLYLSULFANYL-[1,3,4]THIADIAZOL-2-YLAMINE

Chemical Property:

• Vapor Pressure: 0.000419mmHg at 25°C
• Boiling Point: 316.1°Cat760mmHg
• PKA: 2.33±0.10(Predicted)
• Flash Point: 145°C
• PSA: 105.34000
• Density: 1.35g/cm³
• LogP: 1.97960

Purity/Quality:

97% ^*data from raw suppliers

5-(Prop-2-en-1-ylsulfanyl)-1,3,4-thiadiazol-2-amine ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 5-ALLYLSULFANYL-[1,3,4]THIADIAZOL-2-YLAMINE

There total 4 articles about 5-ALLYLSULFANYL-[1,3,4]THIADIAZOL-2-YLAMINE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

2-Amino-5-mercapto-1,3,4-thiadiazole (2349-67-9) + 3-chloroprop-1-ene (107-05-1) → 5-[(prop-2-en-1-yl)sulfanyl]-1,3,4-thiadiazol-2-amine (30062-44-3)

Guidance literature:

With sodium hydrogencarbonate; In ethanol;

DOI:10.1134/S0022476617020184

Reference yield: 49.4%

allyl bromide (106-95-6) + 2-Amino-5-mercapto-1,3,4-thiadiazole (2349-67-9) → 5-[(prop-2-en-1-yl)sulfanyl]-1,3,4-thiadiazol-2-amine (30062-44-3)

Guidance literature:

With potassium hydroxide; In ethanol; at 10 - 20 ℃;

DOI:10.1016/j.molstruc.2020.128507

Reference yield:

2-Amino-5-mercapto-1,3,4-thiadiazole (2349-67-9) → 5-[(prop-2-en-1-yl)sulfanyl]-1,3,4-thiadiazol-2-amine (30062-44-3)

Guidance literature:

With potassium hydroxide;

upstream raw materials:

2-Amino-5-mercapto-1,3,4-thiadiazole

3-chloroprop-1-ene

allyl bromide

Downstream raw materials:

2-allylsulfanyl-[1,3,4]thiadiazolo[3,2-a]pyrimidine-5,7-dione

2-allylsulfanyl-6-benzyl-[1,3,4]thiadiazolo[3,2-a]pyrimidine-5,7-dione

2-allylsulfanyl-6-phenylimidazo[2,1-b][1,3,4]thiadiazole

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