(NE)-N-[1-(4-phenoxyphenyl)ethylidene]hydroxylamine

Base Information

Chemical Name:(NE)-N-[1-(4-phenoxyphenyl)ethylidene]hydroxylamine
CAS No.:6337-25-3
Molecular Formula:C14H13 N O2
Molecular Weight:227.263
Hs Code.:2928000090
NSC Number:39659
Mol file:6337-25-3.mol

Synonyms:NSC39659;6337-25-3;SCHEMBL8438349;NSC-39659

Suppliers and Price of (NE)-N-[1-(4-phenoxyphenyl)ethylidene]hydroxylamine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of (NE)-N-[1-(4-phenoxyphenyl)ethylidene]hydroxylamine

Chemical Property:

Vapor Pressure:6.15E-06mmHg at 25°C
Melting Point:135 °C
Boiling Point:364°C at 760 mmHg
PKA:11.40±0.70(Predicted)
Flash Point:174°C
PSA：41.82000
Density:1.08g/cm³
LogP:3.67710
XLogP3:3.4
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:3
Exact Mass:227.094628657
Heavy Atom Count:17
Complexity:251

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(=NO)C1=CC=C(C=C1)OC2=CC=CC=C2
Isomeric SMILES:C/C(=N\O)/C1=CC=C(C=C1)OC2=CC=CC=C2

Technology Process of (NE)-N-[1-(4-phenoxyphenyl)ethylidene]hydroxylamine

There total 4 articles about (NE)-N-[1-(4-phenoxyphenyl)ethylidene]hydroxylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 5031-78-7
4-phenoxyacetophenone

: 6337-25-3
1-(4-phenoxy-phenyl)-ethanone oxime

Guidance literature:: With hydroxylamine hydrochloride; sodium acetate; In ethanol; water; Reflux;
DOI:10.1016/j.cclet.2021.10.020

Reference yield:

: 108-90-7
chlorobenzene

: 6337-25-3
1-(4-phenoxyphenyl)ethan-1-one oxime

Guidance literature:: Multi-step reaction with 2 steps

1.1: caesium carbonate / dichloromethane / 130 °C

1.2: 130 °C

2.1: hydroxylamine hydrochloride; sodium acetate / ethanol / 80 °C

With hydroxylamine hydrochloride; sodium acetate; caesium carbonate; In ethanol; dichloromethane;
DOI:10.1016/j.molstruc.2022.132670