1,9-Dimethylphenanthrene

Base Information

Chemical Name:1,9-Dimethylphenanthrene
CAS No.:20291-73-0
Molecular Formula:C₁₆H₁₄
Molecular Weight:206.287
Hs Code.:2902909090
DSSTox Substance ID:DTXSID40942430
Nikkaji Number:J957.765C
Wikidata:Q82919442
Mol file:20291-73-0.mol

Synonyms:1,9-dimethylphenanthrene;20291-73-0;DIMETHYLPHENANTHRENE;Phenanthrene, 1,9-dimethyl-;Phenanthrene, dimethyl-;29062-98-4;DTXSID40942430;UGZLIZPBSLIKKG-UHFFFAOYSA-N;FT-0738981

Suppliers and Price of 1,9-Dimethylphenanthrene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
1,9-DIMETHYLPHENANTHRENE 98.00%
5MG
$ 505.47

Total 4 raw suppliers

Chemical Property of 1,9-Dimethylphenanthrene

Chemical Property:

Vapor Pressure:2.89E-05mmHg at 25°C
Boiling Point:367.4°C at 760 mmHg
Flash Point:167°C
PSA：0.00000
Density:1.084g/cm³
LogP:4.60980
XLogP3:5.5
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:0
Exact Mass:206.109550447
Heavy Atom Count:16
Complexity:244

Purity/Quality:

98% ^*data from raw suppliers

1,9-DIMETHYLPHENANTHRENE 98.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=C2C=C(C3=CC=CC=C3C2=CC=C1)C

Technology Process of 1,9-Dimethylphenanthrene

There total 6 articles about 1,9-Dimethylphenanthrene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

: 61161-21-5
2-(1'-methylethenyl)-1-iodobenzene

: C₉H₇BrO₃

: 20291-73-0
1,9-dimethylphenanthrene

Guidance literature:: With trifuran-2-yl-phosphane; palladium diacetate; lithium tert-butoxide; Trimethylacetic acid; In N,N-dimethyl acetamide; at 20 - 120 ℃; for 12.25h; regioselective reaction; Sealed tube;
DOI:10.1021/acs.orglett.1c03517

Reference yield:

: 20291-73-0
1,9-dimethylphenanthrene

Guidance literature:: With selenium; at 340 - 350 ℃;

Reference yield:

: 148517-71-9
1-(2-bromo-6-methylphenyl)ethanone

: 20291-73-0
1,9-dimethylphenanthrene

Guidance literature:: Multi-step reaction with 2 steps

1: selenium(IV) oxide

2: palladium diacetate; trifuran-2-yl-phosphane; lithium tert-butoxide; Trimethylacetic acid / N,N-dimethyl acetamide / 12.25 h / 20 - 120 °C / Sealed tube

With selenium(IV) oxide; trifuran-2-yl-phosphane; palladium diacetate; lithium tert-butoxide; Trimethylacetic acid; In N,N-dimethyl acetamide;
DOI:10.1021/acs.orglett.1c03517