Benzaldehyde 3-chlorophenylhydrazone

Base Information

• Chemical Name: Benzaldehyde 3-chlorophenylhydrazone
• CAS No.: 2989-41-5
• Molecular Formula: C13H11 Cl N2
• Molecular Weight: 230.697
• Mol file: 2989-41-5.mol

Synonyms:Benzaldehyde 3-chlorophenylhydrazone;BRN 1819305;Benzaldehyde, (m-chlorophenyl)hydrazone;2989-41-5;(1E)-1-Benzylidene-2-(3-chlorophenyl)hydrazine;4-15-00-00262 (Beilstein Handbook Reference);SCHEMBL10335995;LS-24975

Chemical Property of Benzaldehyde 3-chlorophenylhydrazone

Chemical Property:

• Vapor Pressure: 0mmHg at 25°C
• Boiling Point: 353.994°C at 760 mmHg
• Flash Point: 167.89°C
• Density: 1.133g/cm³
• XLogP3: 4.2
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 3
• Exact Mass: 230.0610761
• Heavy Atom Count: 16
• Complexity: 224

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC=C(C=C1)C=NNC2=CC(=CC=C2)Cl
• Isomeric SMILES: C1=CC=C(C=C1)/C=N/NC2=CC(=CC=C2)Cl

Technology Process of Benzaldehyde 3-chlorophenylhydrazone

There total 2 articles about Benzaldehyde 3-chlorophenylhydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

m-chlorophenylhydrazine hydrochloride (2312-23-4) + benzaldehyde (100-52-7) → benzaldehyde-(3-chloro-phenylhydrazone) (2989-41-5)

Guidance literature:

m-chlorophenylhydrazine hydrochloride; With triethylamine; In ethanol; water; at 20 ℃; for 0.25h; Darkness;

benzaldehyde; In ethanol; water; at 20 ℃; Darkness;

DOI:10.1016/j.ejmech.2017.09.037

Reference yield:

benzaldehyde (100-52-7) + 3-chlorophenyl hydrazine (14763-20-3) → benzaldehyde-(3-chloro-phenylhydrazone) (2989-41-5)

Guidance literature:

With ammonia;

Reference yield: 83.0%

benzaldehyde-(3-chloro-phenylhydrazone) (2989-41-5) + N,N-dimethyl-formamide (68-12-2,33513-42-7) → N’-(3-chlorophenyl)-N’-formylbenzohydrazide

Guidance literature:

With oxygen; copper(ll) bromide; at 160 ℃;

DOI:10.1039/c7ob00042a

upstream raw materials:

benzaldehyde

3-chlorophenyl hydrazine

m-chlorophenylhydrazine hydrochloride

Downstream raw materials:

tert-butyl 4'-tert-butyl-2'-(3-chlorophenyl)-2-oxo-5'-phenyl-2',4'-dihydrospiro[indoline-3,3'-pyrazole]-1-carboxylate