5-Chloro-2-hydroxy-3-((E)-2-nitroethenyl)benzoic acid

Base Information

Chemical Name:5-Chloro-2-hydroxy-3-((E)-2-nitroethenyl)benzoic acid
CAS No.:111870-28-1
Molecular Formula:C₉H₆ClNO₅
Molecular Weight:243.603
Hs Code.:
Mol file:111870-28-1.mol

Synonyms:111870-28-1;5-Chloro-2-hydroxy-3-((E)-2-nitroethenyl)benzoic acid

Suppliers and Price of 5-Chloro-2-hydroxy-3-((E)-2-nitroethenyl)benzoic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of 5-Chloro-2-hydroxy-3-((E)-2-nitroethenyl)benzoic acid

Chemical Property:

Vapor Pressure:3.3E-09mmHg at 25°C
Boiling Point:458.7°Cat760mmHg
Flash Point:231.2°C
Density:1.628g/cm³
XLogP3:2.5
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:2
Exact Mass:242.9934500
Heavy Atom Count:16
Complexity:314

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=C(C=C(C(=C1C=C[N+](=O)[O-])O)C(=O)O)Cl
Isomeric SMILES:C1=C(C=C(C(=C1/C=C/[N+](=O)[O-])O)C(=O)O)Cl

Technology Process of 5-Chloro-2-hydroxy-3-((E)-2-nitroethenyl)benzoic acid

There total 2 articles about 5-Chloro-2-hydroxy-3-((E)-2-nitroethenyl)benzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.0%

: 75-52-5
nitromethane

: 111870-27-0
5-chloro-3-formyl-2-hydroxybenzoic acid

: 111870-28-1
5-chloro-3-(2-nitroethenyl)salicylic acid

Guidance literature:: With N-butylamine; In acetic acid; for 4h; Heating;

Reference yield:

: 321-14-2
5-chloro-2-hydroxybenzoic acid

: 111870-28-1
5-chloro-3-(2-nitroethenyl)salicylic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 42 percent / NaOH / H₂O / 30 h / Heating

2: 30 percent / n-butylamine / acetic acid / 4 h / Heating

With sodium hydroxide; N-butylamine; In water; acetic acid;

Reference yield:

: 111870-28-1
5-chloro-3-(2-nitroethenyl)salicylic acid

: 111870-34-9
5-Chloro-N-(4-fluoro-phenyl)-3-{[(Z)-4-fluoro-phenylimino]-methyl}-2-hydroxy-benzamide

Guidance literature:: Multi-step reaction with 3 steps

1: SOCl₂ / 0.33 h / Heating

2: 65 percent / triethylamine / benzene / 1 h, 5 deg C; 1 h, room temperature

3: 85 percent / benzene / 6 h / Heating

With thionyl chloride; triethylamine; In benzene;