2-Formylcinchoninic acid 3-thiocarbazone hydrate

Base Information

Chemical Name:2-Formylcinchoninic acid 3-thiocarbazone hydrate
CAS No.:62604-48-2
Molecular Formula:C12H11N5O2S
Molecular Weight:289.313
Hs Code.:

Synonyms:2-Formylcinchoninic acid 3-thiocarbazone hydrate;Cinchoninic acid, 2-formyl-, 3-thiocarbazone, monohydrate;4-Quinolinecarboxylic acid, 2-(((hydrazinothioxomethyl)hydrazono)methyl)-, monohydrate;62604-48-2;C12H11N5O2S.H2O;C12-H11-N5-O2-S.H2-O;LS-53791

Suppliers and Price of 2-Formylcinchoninic acid 3-thiocarbazone hydrate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of 2-Formylcinchoninic acid 3-thiocarbazone hydrate

Chemical Property:

Vapor Pressure:0mmHg at 25°C
Boiling Point:539.295°C at 760 mmHg
Flash Point:279.956°C
Density:1.541g/cm³
XLogP3:-1.3
Hydrogen Bond Donor Count:4
Hydrogen Bond Acceptor Count:6
Rotatable Bond Count:3
Exact Mass:289.06334578
Heavy Atom Count:20
Complexity:403

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C2C(=C1)C(=CC(=N2)C=NNC(=S)NN)C(=O)O
Isomeric SMILES:C1=CC=C2C(=C1)C(=CC(=N2)/C=N/NC(=S)NN)C(=O)O

Technology Process of 2-Formylcinchoninic acid 3-thiocarbazone hydrate

There total 3 articles about 2-Formylcinchoninic acid 3-thiocarbazone hydrate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.1%

: 36783-44-5
2-formylquinoline-4-carboxylic acid

: 2231-57-4
Thiocarbohydrazide

: 62604-48-2
C₁₂H₁₁N₅O₂S

Guidance literature:: In ethanol; at 65 - 70 ℃; for 0.5h;
DOI:10.1007/BF00762028

Reference yield:

: 634-38-8
2-methylquinoline-4-carboxylic acid

: 62604-48-2
C₁₂H₁₁N₅O₂S

Guidance literature:: Multi-step reaction with 2 steps

1: 90.4 percent / SeO₂ / dioxane / 5 h / 100 - 110 °C

2: 79.1 percent / aq. ethanol / 0.5 h / 65 - 70 °C

With selenium(IV) oxide; In 1,4-dioxane; ethanol;
DOI:10.1007/BF00762028