4-Vinylbenzenesulfonamide

Base Information

• Chemical Name: 4-Vinylbenzenesulfonamide
• CAS No.: 2633-64-9
• Molecular Formula: C8H9 N O2 S
• Molecular Weight: 183.231
• Hs Code.: 2935009090
• European Community (EC) Number: 696-150-5
• NSC Number: 133349
• DSSTox Substance ID: DTXSID60299857
• Nikkaji Number: J62.919G
• Wikidata: Q82042544
• Mol file: 2633-64-9.mol

Synonyms:4-Vinylbenzenesulfonamide;2633-64-9;4-ethenylbenzenesulfonamide;4-Sulfonamidostyrene;4-ethenylbenzene-1-sulfonamide;p-styrenesulfonamide;NSC133349;p-sulfonamido styrene;p-Vinylbenzenesulfonamide;4-vinyl-benzenesulphonamide;4-Vinylbenzenesulfonamide #;SCHEMBL393905;Methylen-p-Toluolsulfosaureamid;4-(SULFONAMIDO)STYRENE;SCHEMBL12050255;DTXSID60299857;MFCD00078350;AKOS006345455;NSC 133349;NSC-133349;CS-0091029;FT-0692604;EN300-246650;N16925

Chemical Property of 4-Vinylbenzenesulfonamide

Chemical Property:

• Vapor Pressure: 4.19E-05mmHg at 25°C
• Melting Point: 137-139°C
• Boiling Point: 351.1°C at 760 mmHg
• PKA: 10.10±0.10(Predicted)
• Flash Point: 166.2°C
• PSA: 68.54000
• Density: 1.269g/cm³
• LogP: 2.75810
• XLogP3: 1.2
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 2
• Exact Mass: 183.03539970
• Heavy Atom Count: 12
• Complexity: 245

Purity/Quality:

4-SULFONAMIDOSTYRENE 95.00% ^*data from reagent suppliers

Safty Information:

• Statements: 20/21/22
• Safety Statements: 36/37/39

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C=CC1=CC=C(C=C1)S(=O)(=O)N

Technology Process of 4-Vinylbenzenesulfonamide

There total 8 articles about 4-Vinylbenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

→ 4-vinylbenzenesulfonamide (2633-64-9)

Guidance literature:

Reference yield: 62.0%

4-vinylbenzenesulfonyl chloride (2633-67-2) → 4-vinylbenzenesulfonamide (2633-64-9)

Guidance literature:

With ammonium hydroxide; for 2h;

Reference yield: 56.0%

vinyl acetate (108-05-4,9003-20-7) + 4-bromo-benzenesulfonic acid amide (701-34-8) → 4-vinylbenzenesulfonamide (2633-64-9)

Guidance literature:

With 1,3-bis[(diphenylphosphino)propane]dichloronickel(II); lithium iodide; zinc; at 65 ℃; for 8h; Inert atmosphere; Sealed tube; Green chemistry;

DOI:10.1021/acs.orglett.1c04018

upstream raw materials:

4-(2-bromoethyl)-benzenesulfonamide

2-(4-Aminosulfonylphenyl)ethyl chloride

4-vinylbenzenesulfonyl chloride

sodium 4-styrenesulfonate

Downstream raw materials:

4-(1,2-dibromo-ethyl)-benzenesulfonic acid amide

1-Propyl-3-(p-vinylbenzolsulfonyl)thioharnstoff

1-Phenyl-3-(p-vinylbenzolsulfonyl)harnstoff

1-Allyl-3-(p-vinylbenzolsulfonyl)thioharnstoff