Ethanimidic acid, N-methoxy-, ethyl ester

Base Information

Chemical Name:Ethanimidic acid, N-methoxy-, ethyl ester
CAS No.:21250-85-1
Molecular Formula:C₅H₁₁NO₂
Molecular Weight:117.148
Hs Code.:2925290090
DSSTox Substance ID:DTXSID7066693
Mol file:21250-85-1.mol

Synonyms:Ethanimidic acid, N-methoxy-, ethyl ester;21250-85-1;N-Methoxyethanimidic acid, ethyl ester;DTXSID7066693

Suppliers and Price of Ethanimidic acid, N-methoxy-, ethyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of Ethanimidic acid, N-methoxy-, ethyl ester

Chemical Property:

Vapor Pressure:32.3mmHg at 25°C
Boiling Point:107°Cat760mmHg
Flash Point:20.8°C
PSA：30.82000
Density:0.91g/cm³
LogP:1.00270
XLogP3:1.1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:3
Exact Mass:117.078978594
Heavy Atom Count:8
Complexity:80.5

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CCOC(=NOC)C

Technology Process of Ethanimidic acid, N-methoxy-, ethyl ester

There total 2 articles about Ethanimidic acid, N-methoxy-, ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: 10576-12-2
ethyl acetohydroximate

: 77-78-1
dimethyl sulfate

: 21250-85-1
ethyl-N-methoxy-acetimidate

Guidance literature:: With sodium hydroxide; tetra(n-butyl)ammonium hydrogensulfate; In water; for 1.5h;
DOI:10.1016/S0040-4020(01)88806-2

Reference yield:

: 10576-12-2
ethyl acetohydroximate

: 74-88-4
methyl iodide

: 21250-85-1
ethyl-N-methoxy-acetimidate

Guidance literature:: With sodium methylate; In methanol;

Reference yield:

: 21250-85-1
ethyl-N-methoxy-acetimidate

: 95614-81-6
(S)-3-Hydroxy-N-methoxy-3-phenyl-propionimidic acid ethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) LDA / 1.) THF, -78 deg C, 30 min; 2.) THF, -78 deg C, 5 min

2: 1.) n-BuLi, ZnCl₂, / 1.) THF, -78 deg C, 30 min; 2.) -78 deg C to rt 4 h, rt 30 min

3: 75 percent / anhydrous NaH₂PO₄, 15percent sodium amalgam / methanol / -15 °C

With sodium dihydrogenphosphate; sodium amalgam; n-butyllithium; zinc(II) chloride; lithium diisopropyl amide; In methanol;
DOI:10.1016/S0040-4020(01)88806-2