N-[4-(methanesulfonamido)phenyl]methanesulfonamide

Base Information

• Chemical Name: N-[4-(methanesulfonamido)phenyl]methanesulfonamide
• CAS No.: 33256-34-7
• Molecular Formula: C8H12N2O4S2
• Molecular Weight: 264.326
• NSC Number: 159014
• DSSTox Substance ID: DTXSID60954898
• Wikidata: Q82934334

Synonyms:33256-34-7;N-[4-(methanesulfonamido)phenyl]methanesulfonamide;N-(4-Methanesulfonylamino-phenyl)-methanesulfonamide;N-{4-[(methylsulfonyl)amino]phenyl}methanesulfonamide;n,n'-benzene-1,4-diyldimethanesulfonamide;NSC159014;N,N'-(1,4-Phenylene)dimethanesulfonamide;Oprea1_217058;SCHEMBL12054668;DTXSID60954898;STK981634;AKOS001036939;NSC-159014;N,N'-(benzene-1,4-diyl)dimethanesulfonamide;AH-357/03430016;SR-01000239495;SR-01000239495-1;Z56113896

Chemical Property of N-[4-(methanesulfonamido)phenyl]methanesulfonamide

Chemical Property:

• XLogP3: 0.2
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 6
• Rotatable Bond Count: 4
• Exact Mass: 264.02384922
• Heavy Atom Count: 16
• Complexity: 368

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CS(=O)(=O)NC1=CC=C(C=C1)NS(=O)(=O)C

Technology Process of N-[4-(methanesulfonamido)phenyl]methanesulfonamide

There total 4 articles about N-[4-(methanesulfonamido)phenyl]methanesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 38.0%

N,N′-(cyclohexa-2,5-diene-1,4-diylidene)dimethanesulfonamide (6943-16-4,76165-46-3,76165-47-4) + sodium 4-fluorobenzenesulfinate (824-80-6) → N,N′-[2-(4-fluorobenzenesulfonyl)benzene-1,4-diyl]dimethanesulfonamide + N-(4-fluorobenzenesulfonyl)-N,N′-(benzene-1,4-diyl)dimethanesulfonamide + N,N′-(benzene-1,4-diyl)dimethanesulfonamide (33256-34-7)

Guidance literature:

With acetic acid; at 70 ℃;

DOI:10.1134/S1070428015010078

Reference yield: 16.0%

N,N′-(cyclohexa-2,5-diene-1,4-diylidene)dimethanesulfonamide (6943-16-4,76165-46-3,76165-47-4) + sodium 4-methoxybenzenesulfinate (6462-50-6) → N,N′-[2-(4-methoxybenzenesulfonyl)benzene-1,4-diyl]dimethanesulfonamide + N-(4-methoxybenzenesulfonyl)-N,N′-(benzene-1,4-diyl)dimethanesulfonamide + N,N′-(benzene-1,4-diyl)dimethanesulfonamide (33256-34-7)

Guidance literature:

With acetic acid; at 70 ℃;

DOI:10.1134/S1070428015010078

Reference yield:

N,N′-(cyclohexa-2,5-diene-1,4-diylidene)dimethanesulfonamide (6943-16-4,76165-46-3,76165-47-4) + sodium 4-methylbenzenesulfinate (824-79-3) → N,N′-[2-(4-methylbenzenesulfonyl)benzene-1,4-diyl]dimethanesulfonamide + N-(4-methylbenzenesulfonyl)-N,N′-(benzene-1,4-diyl)dimethanesulfonamide + N,N′-(benzene-1,4-diyl)dimethanesulfonamide (33256-34-7)

Guidance literature:

With acetic acid; at 70 ℃;

DOI:10.1134/S1070428015010078

upstream raw materials:

N,N′-(cyclohexa-2,5-diene-1,4-diylidene)dimethanesulfonamide

sodium 4-methylbenzenesulfinate

sodium 4-methoxybenzenesulfinate

sodium 4-fluorobenzenesulfinate

Downstream raw materials:

2,3,5,6-tetrachloro-N,N'-bis(methylsulfonyl)-p-benzoquinone diimine

2,3,5,6,-tetrachloro-N,N'-bis(methylsulfonyl)-p-phenylenediamine

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