Benzenecarbohydrazonoyl chloride, 4-bromo-N-phenyl-

Base Information

Chemical Name:Benzenecarbohydrazonoyl chloride, 4-bromo-N-phenyl-
CAS No.:25939-12-2
Molecular Formula:C13H10 Br Cl N2
Molecular Weight:309.593
Hs Code.:2928000090
ChEMBL ID:CHEMBL150401
Mol file:25939-12-2.mol

Synonyms:4-Bromobenzoyl chloride phenylhydrazone;BRN 0959324;Benzenecarbohydrazonoyl chloride, 4-bromo-N-phenyl-;BENZOYL CHLORIDE, p-BROMO-, PHENYLHYDRAZONE;C13H10BrClN2;25939-12-2;CHEMBL150401;LS-42594;N(4-bromo-benzimidoyl chloride)Phenylamine

Suppliers and Price of Benzenecarbohydrazonoyl chloride, 4-bromo-N-phenyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
4-BROMOBENZOYL CHLORIDE PHENYLHYDRAZONE 95.00%
5MG
$ 497.50

Total 3 raw suppliers

Chemical Property of Benzenecarbohydrazonoyl chloride, 4-bromo-N-phenyl-

Chemical Property:

Vapor Pressure:0mmHg at 25°C
Boiling Point:384.5°Cat760mmHg
Flash Point:186.3°C
PSA：24.39000
Density:1.43g/cm³
LogP:4.53460
XLogP3:5.3
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:3
Exact Mass:307.97159
Heavy Atom Count:17
Complexity:256

Purity/Quality:

99% ^*data from raw suppliers

4-BROMOBENZOYL CHLORIDE PHENYLHYDRAZONE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)NN=C(C2=CC=C(C=C2)Br)Cl
Isomeric SMILES:C1=CC=C(C=C1)N/N=C(/C2=CC=C(C=C2)Br)\Cl

Technology Process of Benzenecarbohydrazonoyl chloride, 4-bromo-N-phenyl-

There total 8 articles about Benzenecarbohydrazonoyl chloride, 4-bromo-N-phenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 16917-42-3
4-bromobenzaldehyde phenylhydrazone

: 25939-12-2
4-bromo-N-phenylbenzohydrazonoyl chloride

Guidance literature:: With N-chloro-succinimide; dimethylsulfide; In dichloromethane; at -78 - 20 ℃; for 16.5h; Schlenk technique; Inert atmosphere;
DOI:10.1002/anie.202015058

Reference yield:

: 25938-97-0
4-bromo-N'-phenylbenzohydrazide

: 25939-12-2
4-bromo-N-phenylbenzohydrazonoyl chloride

Guidance literature:: With tetrachloromethane; triphenylphosphine; In acetonitrile; at 20 ℃; Inert atmosphere;
DOI:10.1021/acs.orglett.7b01961

Reference yield:

: 100-63-0
phenylhydrazine

: 25939-12-2
4-bromo-N-phenylbenzohydrazonoyl chloride

Guidance literature:: Multi-step reaction with 2 steps

1: ethanol; water / 1 h / 20 °C

2: N-chlorosuccinimide-dimethylsulfide complex / dichloromethane / -40 - 0 °C

With N-chlorosuccinimide-dimethylsulfide complex; In ethanol; dichloromethane; water;
DOI:10.1007/s00706-011-0618-z