4-methyl-2-phenyl-2-(prop-2-en-1-yloxy)morpholine hydrochloride (1:1)

Base Information

• Chemical Name: 4-methyl-2-phenyl-2-(prop-2-en-1-yloxy)morpholine hydrochloride (1:1)
• CAS No.: 124497-81-0
• Molecular Formula: C₁₄H₁₉NO₂*ClH
• Molecular Weight: 269.771
• Mol file: 124497-81-0.mol

Synonyms:Morpholine,4-methyl-2-phenyl-2-(2-propenyloxy)-, hydrochloride (9CI)

Chemical Property of 4-methyl-2-phenyl-2-(prop-2-en-1-yloxy)morpholine hydrochloride (1:1)

Chemical Property:

• Vapor Pressure: 0.000198mmHg at 25°C
• Boiling Point: 327.7°C at 760 mmHg
• Flash Point: 111.6°C

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-methyl-2-phenyl-2-(prop-2-en-1-yloxy)morpholine hydrochloride (1:1)

There total 2 articles about 4-methyl-2-phenyl-2-(prop-2-en-1-yloxy)morpholine hydrochloride (1:1) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

4-Methyl-2-phenyl-morpholin-2-ol; hydrochloride (124497-72-9) + allyl alcohol (107-18-6) → 2-Allyloxy-4-methyl-2-phenyl-morpholine; hydrochloride (124497-81-0)

Guidance literature:

With acid;

DOI:10.1016/0223-5234(89)90112-8

Reference yield:

α-bromoacetophenone (70-11-1) → 2-Allyloxy-4-methyl-2-phenyl-morpholine; hydrochloride (124497-81-0)

Guidance literature:

Multi-step reaction with 2 steps

1: 72 percent / 2.) ethereal hydrogen chloride / diethyl ether / Ambient temperature

2: 72 percent / acid

With hydrogenchloride; In diethyl ether;

DOI:10.1016/0223-5234(89)90112-8

upstream raw materials:

4-Methyl-2-phenyl-morpholin-2-ol; hydrochloride

allyl alcohol

α-bromoacetophenone