Benzenamine, 4,5-dimethoxy-2,3-dimethyl-

Base Information

Chemical Name:Benzenamine, 4,5-dimethoxy-2,3-dimethyl-
CAS No.:100132-28-3
Molecular Formula:C10H15NO2
Molecular Weight:181.235
Hs Code.:
DSSTox Substance ID:DTXSID30456137
Nikkaji Number:J826.472D
Wikidata:Q82278359
Mol file:100132-28-3.mol

Synonyms:Benzenamine, 4,5-dimethoxy-2,3-dimethyl-;100132-28-3;4,5-dimethoxy-2,3-dimethylaniline;DTXSID30456137;2,3-Dimethyl-4,5-dimethoxyaniline

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzenamine, 4,5-dimethoxy-2,3-dimethyl-

Chemical Property:

XLogP3:1.9
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:2
Exact Mass:181.110278721
Heavy Atom Count:13
Complexity:163

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=C(C(=C(C=C1N)OC)OC)C

Technology Process of Benzenamine, 4,5-dimethoxy-2,3-dimethyl-

There total 8 articles about Benzenamine, 4,5-dimethoxy-2,3-dimethyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 153709-76-3
1,2-dimethoxy-3,4-dimethyl-5-nitrobenzene

: 100132-28-3
4,5-dimethoxy-2,3-dimethylaniline

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethanol; under 912 Torr; Ambient temperature;
DOI:10.1002/hlca.19930760709

Reference yield:

: 118538-99-1
2-methoxy-3,4-dimethyl-5-nitrophenol

: 100132-28-3
4,5-dimethoxy-2,3-dimethylaniline

Guidance literature:: Multi-step reaction with 2 steps

2: H₂ / Pd/C

With hydrogen; palladium on activated charcoal;
DOI:10.1039/C39890001468

Reference yield:

: 4463-33-6
1,2-dimethoxy-3-methylbenzene

: 100132-28-3
4,5-dimethoxy-2,3-dimethylaniline

Guidance literature:: Multi-step reaction with 4 steps

1.1: 88 percent / NBS / acetonitrile / 3 h / 25 °C

2.1: BuLi / tetrahydrofuran / -78 °C

2.2: 86 percent / tetrahydrofuran / -78 - 25 °C

3.1: 76 percent / HNO₃ / acetic anhydride; acetic acid / 0 °C

4.1: 96 percent / H₂ / 10 percent Pd/C / methanol

With N-Bromosuccinimide; n-butyllithium; hydrogen; nitric acid; palladium on activated charcoal; In tetrahydrofuran; methanol; acetic anhydride; acetic acid; acetonitrile; 1.1: Bromination / 2.1: Metallation / 2.2: Methylation / 3.1: Nitration / 4.1: Catalytic hydrogenation;
DOI:10.1016/S0040-4039(99)01418-5