2H-Azirine, 3-(3-butenyl)-2-methyl-2-phenyl-

Base Information

Chemical Name:2H-Azirine, 3-(3-butenyl)-2-methyl-2-phenyl-
CAS No.:100589-87-5
Molecular Formula:C₁₃H₁₅N
Molecular Weight:185.269
Hs Code.:
DSSTox Substance ID:DTXSID20541127

Synonyms:100589-87-5;2H-Azirine, 3-(3-butenyl)-2-methyl-2-phenyl-;3-but-3-enyl-2-methyl-2-phenylazirine;DTXSID20541127;3-(But-3-en-1-yl)-2-methyl-2-phenyl-2H-azirene;3-(But-3-en-1-yl)-2-methyl-2-phenyl-2H-azirine

Suppliers and Price of 2H-Azirine, 3-(3-butenyl)-2-methyl-2-phenyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2H-Azirine, 3-(3-butenyl)-2-methyl-2-phenyl-

Chemical Property:

XLogP3:2.8
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:4
Exact Mass:185.120449483
Heavy Atom Count:14
Complexity:248

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1(C(=N1)CCC=C)C2=CC=CC=C2

Technology Process of 2H-Azirine, 3-(3-butenyl)-2-methyl-2-phenyl-

There total 2 articles about 2H-Azirine, 3-(3-butenyl)-2-methyl-2-phenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 100632-32-4
1-(tert-Butyl-dimethyl-silanyl)-2-methyl-3-methylene-2-phenyl-aziridine

: 100589-87-5
3-but-3-enyl-2-methyl-2-phenyl-2H-azirine

Guidance literature:: Multi-step reaction with 2 steps

1: tetrahydrofuran; H₂O / 4 h

2: 1.) n BuLi / 1.) THF, -60 deg C

With n-butyllithium; In tetrahydrofuran; water;
DOI:10.1016/S0040-4039(00)98123-1

Reference yield:

: 100589-91-1
3-[(tert-Butyl-dimethyl-silanyl)-methyl]-2-methyl-2-phenyl-2H-azirine

: 100589-87-5
3-but-3-enyl-2-methyl-2-phenyl-2H-azirine

Guidance literature:: Multi-step reaction with 2 steps

1: CsF / H₂O

2: 1.) n BuLi / 1.) THF, -60 deg C

With n-butyllithium; cesium fluoride; In water;
DOI:10.1016/S0040-4039(00)98123-1

Reference yield:

: 100589-87-5
3-but-3-enyl-2-methyl-2-phenyl-2H-azirine

: 98-86-2
acetophenone

: 110775-36-5
3-but-3-enyl-2-methyl-2,5-diphenyl-2H-pyrrole

Guidance literature:: With sodium hydride; Yield given. Multistep reaction; 1.) DMSO, 20 deg C, 2 h, 2.) DMSO, from 20 deg C to 35 deg C, 71 h;
DOI:10.1021/jo00234a009