1-[Bis(trimethylsilyl)methyl]-1-fluoro-3,3,3-trimethyl-1-phenyldisiloxane

Base Information

• Chemical Name: 1-[Bis(trimethylsilyl)methyl]-1-fluoro-3,3,3-trimethyl-1-phenyldisiloxane
• CAS No.: 101069-19-6
• Molecular Formula: C16H33FOSi4
• Molecular Weight: 372.778
• DSSTox Substance ID: DTXSID50548700
• Mol file: 101069-19-6.mol

Synonyms:101069-19-6;DTXSID50548700;1-[Bis(trimethylsilyl)methyl]-1-fluoro-3,3,3-trimethyl-1-phenyldisiloxane

Chemical Property of 1-[Bis(trimethylsilyl)methyl]-1-fluoro-3,3,3-trimethyl-1-phenyldisiloxane

Chemical Property:

• PSA: 9.23000
• LogP: 5.28180
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 6
• Exact Mass: 372.15924997
• Heavy Atom Count: 22
• Complexity: 350

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C[Si](C)(C)C([Si](C)(C)C)[Si](C1=CC=CC=C1)(O[Si](C)(C)C)F

Technology Process of 1-[Bis(trimethylsilyl)methyl]-1-fluoro-3,3,3-trimethyl-1-phenyldisiloxane

There total 2 articles about 1-[Bis(trimethylsilyl)methyl]-1-fluoro-3,3,3-trimethyl-1-phenyldisiloxane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

[Difluoro-(tris-trimethylsilanyl-methyl)-silanyl]-benzene (91153-51-4) → <3-Fluor-1,1,1-trimethyl-3-bis(trimethylsilyl)methyl-3-phenyl>-1,3-disiloxan (101069-19-6) + 1-Hydroxy-1-bis(trimethylsilyl)methyl-1-phenyl-3,3,3-trimethyl-1,3-disiloxan (101069-22-1)

Guidance literature:

With potassium hydroxide; In 1,4-dioxane; for 2h; Heating;

Reference yield:

[Difluoro-(tris-trimethylsilanyl-methyl)-silanyl]-benzene (91153-51-4) → <3-Fluor-1,1,1-trimethyl-3-bis(trimethylsilyl)methyl-3-phenyl>-1,3-disiloxan (101069-19-6)

Guidance literature:

With potassium hydroxide; In water; at 80 - 100 ℃;

DOI:10.1016/0022-328X(87)87123-1

Reference yield: 85.0%

chloro-trimethyl-silane (75-77-4) + <3-Fluor-1,1,1-trimethyl-3-bis(trimethylsilyl)methyl-3-phenyl>-1,3-disiloxan (101069-19-6) → 1-fluor-1-phenyl-1-tris(trimethylsilyl)methyl-3,3,3-trimethyl-1,3-disiloxan (113330-62-4)

Guidance literature:

With methyllithium; In tetrahydrofuran; for 2h; Heating;

DOI:10.1016/0022-328X(87)87123-1

upstream raw materials:

[Difluoro-(tris-trimethylsilanyl-methyl)-silanyl]-benzene

Downstream raw materials:

1-fluor-1-phenyl-1-tris(trimethylsilyl)methyl-3,3,3-trimethyl-1,3-disiloxan

1-Hydroxy-1-bis(trimethylsilyl)methyl-1-phenyl-3,3,3-trimethyl-1,3-disiloxan

bromobenzene

1,1,1,5,5,5-hexamethyl-3-phenyl-3-bis(trimethylsilyl)methyl-1,3,5-trisiloxane

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