9H-Thioxanthen-9-one, 1-[[2-(dimethylamino)ethyl]amino]-4-(hydroxymethyl)-7-[[(4-methylphenyl )sulfonyl]oxy]-

Base Information

Chemical Name:9H-Thioxanthen-9-one, 1-[[2-(dimethylamino)ethyl]amino]-4-(hydroxymethyl)-7-[[(4-methylphenyl )sulfonyl]oxy]-
CAS No.:101339-44-0
Molecular Formula:C25H26N2O5S2
Molecular Weight:498.61400
Hs Code.:

Synonyms:1-{[2-(dimethylamino)ethyl]amino}-4-(hydroxymethyl)-7-(toluenesulfonyloxy)-9H-thioxanthen-9-one;

Suppliers and Price of 9H-Thioxanthen-9-one, 1-[[2-(dimethylamino)ethyl]amino]-4-(hydroxymethyl)-7-[[(4-methylphenyl )sulfonyl]oxy]-

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 9H-Thioxanthen-9-one, 1-[[2-(dimethylamino)ethyl]amino]-4-(hydroxymethyl)-7-[[(4-methylphenyl )sulfonyl]oxy]-

Chemical Property:

Melting Point:175-176 °C(Solv: methanol (67-56-1))
Boiling Point:734.7±60.0 °C(Predicted)
PSA：132.56000
Density:1.377±0.06 g/cm3(Predicted)
LogP:5.11040

Purity/Quality:

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Technology Process of 9H-Thioxanthen-9-one, 1-[[2-(dimethylamino)ethyl]amino]-4-(hydroxymethyl)-7-[[(4-methylphenyl )sulfonyl]oxy]-

There total 9 articles about 9H-Thioxanthen-9-one, 1-[[2-(dimethylamino)ethyl]amino]-4-(hydroxymethyl)-7-[[(4-methylphenyl )sulfonyl]oxy]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 86456-32-8
1-<<2-(dimethylamino)ethyl>amino>-7-(toluenesulfonyloxy)-9H-thioxanthen-9-one

: 101339-44-0
1-<<2-(dimethylamino)ethyl>amino>-4-(hydroxymethyl)-7-(toluenesulfonyloxy)-9H-thioxanthen-9-one

Guidance literature:: With acetic acid; at 80 ℃; for 72h;
DOI:10.1021/jm00396a040

Reference yield:

: 86456-31-7
1-<<2-(dimethylamino)ethyl>amino>-7-hydroxy-9H-thioxanthen-9-one

: 101339-44-0
1-<<2-(dimethylamino)ethyl>amino>-4-(hydroxymethyl)-7-(toluenesulfonyloxy)-9H-thioxanthen-9-one

Guidance literature:: Multi-step reaction with 2 steps

1: 87 percent / pyridine / 0.5 h / Ambient temperature

2: 66 percent / aq. AcOH / 72 h / 80 °C

With acetic acid; In pyridine;
DOI:10.1021/jm00396a040

Reference yield:

: 98-59-9
p-toluenesulfonyl chloride

: 101339-44-0
1-<<2-(dimethylamino)ethyl>amino>-4-(hydroxymethyl)-7-(toluenesulfonyloxy)-9H-thioxanthen-9-one

Guidance literature:: Multi-step reaction with 2 steps

1: 87 percent / pyridine / 0.5 h / Ambient temperature

2: 66 percent / aq. AcOH / 72 h / 80 °C

With acetic acid; In pyridine;
DOI:10.1021/jm00396a040