Acenaphthylene, 4,7-bis(1,1-dimethylethyl)-1,2-dihydro-

Base Information

Chemical Name:Acenaphthylene, 4,7-bis(1,1-dimethylethyl)-1,2-dihydro-
CAS No.:10239-86-8
Molecular Formula:C20H26
Molecular Weight:266.426
Hs Code.:
DSSTox Substance ID:DTXSID60384297
Nikkaji Number:J1.351.432A
Wikidata:Q82176324
Mol file:10239-86-8.mol

Synonyms:4,7-ditert-butyl-1,2-dihydroacenaphthylene;10239-86-8;Acenaphthylene, 4,7-bis(1,1-dimethylethyl)-1,2-dihydro-;Maybridge1_002139;4,7-di-t-butyl-acenaphthene;4,7-Di-tert-butylacenaphthene;HMS547J05;DTXSID60384297

Suppliers and Price of Acenaphthylene, 4,7-bis(1,1-dimethylethyl)-1,2-dihydro-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Acenaphthylene, 4,7-bis(1,1-dimethylethyl)-1,2-dihydro-

Chemical Property:

Melting Point:162.5-163.5 °C
Boiling Point:358-360 °C(Press: 758 Torr)
PSA：0.00000
Density:0.993±0.06 g/cm3(Predicted)
LogP:5.53340
XLogP3:6.8
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:2
Exact Mass:266.203450829
Heavy Atom Count:20
Complexity:319

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(C)(C)C1=CC2=CC(=CC3=C2C(=C1)CC3)C(C)(C)C

Technology Process of Acenaphthylene, 4,7-bis(1,1-dimethylethyl)-1,2-dihydro-

There total 1 articles about Acenaphthylene, 4,7-bis(1,1-dimethylethyl)-1,2-dihydro- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 7446-70-0
aluminium trichloride

: 35210-35-6
5-(tert-butyl)-1,2-dihydroacenaphthylene

: 55939-14-5
4-tert-butyl-acenaphthene

: 10239-86-8
4,7-di-tert-butyl-1,2-dihydroacenaphthylene

: 83-32-9
acenaphthene

Guidance literature:: DOI:10.1039/jr9520002730

Reference yield:

: 10239-86-8
4,7-di-tert-butyl-1,2-dihydroacenaphthylene

: F₆P^(1-)*C₂₄H₃₂O₈*C₃₁H₃₅N₄O₂⁽¹⁺⁾

Guidance literature:: Multi-step reaction with 5 steps

1: sodium dichromate; acetic acid / 1 h / 100 °C

2: ethanol / 2 h / Reflux

3: tetrakis(actonitrile)copper(I) hexafluorophosphate; 2,6-dimethylpyridine / dichloromethane / 24 h / 20 °C

4: 120 h / 20 °C

5: dichloromethane / 20 °C

With 2,6-dimethylpyridine; sodium dichromate; tetrakis(actonitrile)copper(I) hexafluorophosphate; acetic acid; In ethanol; dichloromethane;
DOI:10.1002/chem.201604783

Reference yield:

: 10239-86-8
4,7-di-tert-butyl-1,2-dihydroacenaphthylene

: C₃₀H₃₂N₄O₂

Guidance literature:: Multi-step reaction with 3 steps

1: sodium dichromate; acetic acid / 1 h / 100 °C

2: ethanol / 2 h / Reflux

3: tetrakis(actonitrile)copper(I) hexafluorophosphate; 2,6-dimethylpyridine / dichloromethane / 24 h / 20 °C

With 2,6-dimethylpyridine; sodium dichromate; tetrakis(actonitrile)copper(I) hexafluorophosphate; acetic acid; In ethanol; dichloromethane;
DOI:10.1002/chem.201604783