N-m-Chlorobenzylethylenediamine

Base Information

• Chemical Name: N-m-Chlorobenzylethylenediamine
• CAS No.: 102450-75-9
• Molecular Formula: C9H13ClN2
• Molecular Weight: 184.669
• Hs Code.: 2921590090
• Mol file: 102450-75-9.mol

Synonyms:(2-aminoethyl)[(3-chlorophenyl)methyl]amine;N-(3-CHLOROBENZYL)ETHANE-1,2-DIAMINE;N-(3-chloro-benzyl)-ethylenediamine;N-(3-Chlor-benzyl)-aethylendiamin;

Chemical Property of N-m-Chlorobenzylethylenediamine

Chemical Property:

• Boiling Point: 293℃
• Flash Point: 131℃
• PSA: 38.05000
• Density: 1.131
• LogP: 2.47950

Purity/Quality:

97% ^*data from raw suppliers

N-(3-Chlorobenzyl)ethane-1,2-diamine ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of N-m-Chlorobenzylethylenediamine

There total 4 articles about N-m-Chlorobenzylethylenediamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

m-Chlorobenzaldehyde (587-04-2) + ethylenediamine (107-15-3,85404-18-8) → N-(3-chloro-benzyl)-ethylenediamine (102450-75-9)

Guidance literature:

m-Chlorobenzaldehyde; ethylenediamine; In methanol; Cooling with ice;

With sodium tetrahydroborate; In methanol; at 0 - 20 ℃;

DOI:10.1016/j.bmc.2011.08.054

Reference yield:

ethylenediamine (107-15-3,85404-18-8) + 1-Chloro-3-chloromethyl-benzene (620-20-2,130468-19-8) → N-(3-chloro-benzyl)-ethylenediamine (102450-75-9)

Guidance literature:

ethylenediamine; With lithium; at 110 ℃; for 1h; Inert atmosphere; Schlenk technique;

1-Chloro-3-chloromethyl-benzene; In toluene; Inert atmosphere; Schlenk technique;

DOI:10.1016/j.ica.2016.05.027

Reference yield:

N,N'-(ethane-1,2-diyl)bis(1-(3-chlorophenyl)methanimine) (109886-97-7) → N-(3-chloro-benzyl)-ethylenediamine (102450-75-9)

Guidance literature:

With formic acid;

upstream raw materials:

N,N'-(ethane-1,2-diyl)bis(1-(3-chlorophenyl)methanimine)

m-Chlorobenzaldehyde

ethylenediamine

1-Chloro-3-chloromethyl-benzene

Downstream raw materials:

1-benzyl-1H-benzo[d]imidazole-2-carbaldehyde

1-(3-chlorobenzyl)-2-(nitromethylene)imidazolidine

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