N-[(3-CHLOROPHENYL)METHYLENE]-N-(2-([(3-CHLOROPHENYL)METHYLENE]AMINO)ETHYL)AMINE

Base Information

• Chemical Name: N-[(3-CHLOROPHENYL)METHYLENE]-N-(2-([(3-CHLOROPHENYL)METHYLENE]AMINO)ETHYL)AMINE
• CAS No.: 109886-97-7
• Molecular Formula: C₁₆H₁₄Cl₂N₂
• Molecular Weight: 305.207
• Mol file: 109886-97-7.mol

Synonyms:N,N'-(ethane-1,2-diyl)bis(1-(3-chlorophenyl)methanimine)

Chemical Property of N-[(3-CHLOROPHENYL)METHYLENE]-N-(2-([(3-CHLOROPHENYL)METHYLENE]AMINO)ETHYL)AMINE

Chemical Property:

Purity/Quality:

N1,N2-BIS((3-CHLOROPHENYL)METHYLENE)-1,2-ETHANEDIAMINE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of N-[(3-CHLOROPHENYL)METHYLENE]-N-(2-([(3-CHLOROPHENYL)METHYLENE]AMINO)ETHYL)AMINE

There total 1 articles about N-[(3-CHLOROPHENYL)METHYLENE]-N-(2-([(3-CHLOROPHENYL)METHYLENE]AMINO)ETHYL)AMINE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

m-Chlorobenzaldehyde (587-04-2) + ethylenediamine (107-15-3,85404-18-8) → N,N'-(ethane-1,2-diyl)bis(1-(3-chlorophenyl)methanimine) (109886-97-7)

Guidance literature:

In ethanol; at 20 ℃; for 3h;

DOI:10.1039/c9ob01331h

Reference yield: 75.0%

N,N'-(ethane-1,2-diyl)bis(1-(3-chlorophenyl)methanimine) (109886-97-7) → N1,N2-bis(3-chlorobenzyl)ethane-1,2-diamine (108896-77-1)

Guidance literature:

With sodium tetrahydroborate; sodium hydroxide; In methanol; dichloromethane; at 15 - 18 ℃; for 5h;

DOI:10.5012/jkcs.2013.57.2.227

Reference yield: 53.0%

tetrakis(actonitrile)copper(I) hexafluorophosphate (64443-05-6) + N,N'-(ethane-1,2-diyl)bis(1-(3-chlorophenyl)methanimine) (109886-97-7) → C32H28Cl4CuN4(1+)*F6P(1-)

Guidance literature:

In dichloromethane; at 25 ℃; Schlenk technique; Inert atmosphere;

DOI:10.1039/c9ob01331h

upstream raw materials:

m-Chlorobenzaldehyde

ethylenediamine

Downstream raw materials:

N₁,N₂-bis(3-chlorobenzyl)ethane-1,2-diamine

N-(3-chloro-benzyl)-ethylenediamine

1,5-Bis-(3-chloro-benzyl)-[1,3,5]triazepane-2,4-dione

1,5-Bis-(3-chloro-benzyl)-4-thioxo-[1,3,5]triazepan-2-one

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