Technology Process of Phenyl buta-2,3-dienoate
There total 7 articles about Phenyl buta-2,3-dienoate which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
((triphenyl)-λ5-phosphanylidene)acetic acid phenyl ester;
With
triethylamine;
In
dichloromethane;
at 20 ℃;
for 0.0833333h;
Inert atmosphere;
acetyl chloride;
In
dichloromethane;
at 20 ℃;
for 0.333333h;
Inert atmosphere;
DOI:10.1021/acs.joc.6b01446
- Guidance literature:
-
With
potassium carbonate; 2-chloropyridinium iodide;
In
dichloromethane;
at 20 ℃;
for 4h;
DOI:10.1007/s00706-018-2175-1
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 64 percent / toluene / 15 h / Ambient temperature
2: 1.) NEt3 / 1.) CH2Cl2, RT, 2.) CH2Cl2, RT, 30 min
With
triethylamine;
In
toluene;