N-(2,3-dichlorophenyl)benzamide

Base Information

Chemical Name:N-(2,3-dichlorophenyl)benzamide
CAS No.:10286-77-8
Molecular Formula:C13H9Cl2NO
Molecular Weight:266.12300
Hs Code.:2924299090
European Community (EC) Number:666-705-6
DSSTox Substance ID:DTXSID40356891
Wikidata:Q82136520
ChEMBL ID:CHEMBL2234177
Mol file:10286-77-8.mol

Synonyms:N-(2,3-dichlorophenyl)benzamide;10286-77-8;CBMicro_009679;SCHEMBL9621459;CHEMBL2234177;DTXSID40356891;SMSF0005392;STK085066;N~1~-(2,3-dichlorophenyl)benzamide;AKOS000436848;CB12500;BIM-0009761.P001;CS-0329819;AN-652/40847955

Suppliers and Price of N-(2,3-dichlorophenyl)benzamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Sigma-Aldrich
2',3'-DICHLOROBENZANILIDE Aldrich
250mg
$ 57.00

American Custom Chemicals Corporation
2',3'-DICHLOROBENZANILIDE 95.00%
5MG
$ 495.25

Total 3 raw suppliers

Chemical Property of N-(2,3-dichlorophenyl)benzamide

Chemical Property:

PSA：32.59000
LogP:4.62970
XLogP3:3.7
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:2
Exact Mass:265.0061193
Heavy Atom Count:17
Complexity:266

Purity/Quality:

98%,99%, ^*data from raw suppliers

2',3'-DICHLOROBENZANILIDE Aldrich ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)C(=O)NC2=C(C(=CC=C2)Cl)Cl

Technology Process of N-(2,3-dichlorophenyl)benzamide

There total 6 articles about N-(2,3-dichlorophenyl)benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

: 67055-91-8
N-(m-Chlorophenyl)benzohydroxamic acid

: 10286-77-8
N-(2,3-dichlorophenyl)benzamide

: 6626-75-1
N-(2,5-dichlorophenyl)benzamide

Guidance literature:: With thionyl chloride; In diethyl ether; for 1h; T < 5 deg C;

Reference yield:

: 98-88-4
benzoyl chloride

: 608-27-5
2,3-dichloroaniline

: 10286-77-8
N-(2,3-dichlorophenyl)benzamide

Guidance literature:: With triethylamine; In dichloromethane; at 0 - 20 ℃; for 2h;
DOI:10.1039/d0gc02294b

Reference yield:

: 10468-17-4
N-(3-chlorophenyl)hydroxylamine

: 10286-77-8
N-(2,3-dichlorophenyl)benzamide

Guidance literature:: Multi-step reaction with 2 steps

1: NaHCO₃ / diethyl ether; H₂O / 1 h / T < 5 deg C; or in benzene

2: 25 percent / SOCl₂ / diethyl ether / 1 h / T < 5 deg C

With thionyl chloride; sodium hydrogencarbonate; In diethyl ether; water;