Propanamide, N,2,2-trimethyl-3-[(phenylmethyl)seleno]-

Base Information

Chemical Name:Propanamide, N,2,2-trimethyl-3-[(phenylmethyl)seleno]-
CAS No.:103003-80-1
Molecular Formula:C₁₃H₁₉NOSe
Molecular Weight:284.26
Hs Code.:
Mol file:103003-80-1.mol

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Propanamide, N,2,2-trimethyl-3-[(phenylmethyl)seleno]-

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Propanamide, N,2,2-trimethyl-3-[(phenylmethyl)seleno]-

There total 4 articles about Propanamide, N,2,2-trimethyl-3-[(phenylmethyl)seleno]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 103003-93-6
3-Benzylselanyl-2,2-dimethyl-propionyl chloride

: 74-89-5
methylamine

: 103003-80-1
N-methyl-3-(benzylseleno)-2,2-dimethylpropionamide

Guidance literature:: With oxalyl dichloride; In dichloromethane; water; at 0 ℃; for 1h; Yield given;
DOI:10.1021/jo00365a025

Reference yield:

: 16645-12-8
benzyl selenol

: 103003-80-1
N-methyl-3-(benzylseleno)-2,2-dimethylpropionamide

Guidance literature:: Multi-step reaction with 4 steps

1: 95 percent / 48percent aq. HBr / CH₂Cl₂ / 45 °C

2: 1.) LDA / 1.) THF, RT, 1 h, 2.) THF, RT, 2 h

3: oxalyl chloride / 0.75 h

4: oxalyl chloride / CH₂Cl₂; H₂O / 1 h / 0 °C

With oxalyl dichloride; hydrogen bromide; lithium diisopropyl amide; In dichloromethane; water;
DOI:10.1021/jo00365a025

Reference yield:

: 103003-84-5
bromomethyl benzyl selenide

: 103003-80-1
N-methyl-3-(benzylseleno)-2,2-dimethylpropionamide

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) LDA / 1.) THF, RT, 1 h, 2.) THF, RT, 2 h

2: oxalyl chloride / 0.75 h

3: oxalyl chloride / CH₂Cl₂; H₂O / 1 h / 0 °C

With oxalyl dichloride; lithium diisopropyl amide; In dichloromethane; water;
DOI:10.1021/jo00365a025