5-Methyl-3-phenylhexan-2-one

Base Information

Chemical Name:5-Methyl-3-phenylhexan-2-one
CAS No.:103392-12-7
Molecular Formula:C13H18O
Molecular Weight:190.285
Hs Code.:
DSSTox Substance ID:DTXSID70522901
Mol file:103392-12-7.mol

Synonyms:103392-12-7;5-methyl-3-phenyl-2-Hexanone;5-Methyl-3-phenylhexan-2-one;SCHEMBL2120942;C5-Methyl-3-phenyl-2-hexanone;DTXSID70522901;ZKEQCFAVZIDBCV-UHFFFAOYSA-N;AKOS015814474

Suppliers and Price of 5-Methyl-3-phenylhexan-2-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of 5-Methyl-3-phenylhexan-2-one

Chemical Property:

XLogP3:3.3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:4
Exact Mass:190.135765193
Heavy Atom Count:14
Complexity:178

Purity/Quality:: 98%min ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC(C)CC(C1=CC=CC=C1)C(=O)C

Technology Process of 5-Methyl-3-phenylhexan-2-one

There total 9 articles about 5-Methyl-3-phenylhexan-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 78-77-3
Isobutyl bromide

: 63866-06-8
1-Phenyl-2-propanone Dianion

: 103392-12-7
5-Methyl-3-phenyl-2-hexanone

Guidance literature:: In tetrahydrofuran; for 4h; Ambient temperature;
DOI:10.1021/jo00166a004

Reference yield:

: 605680-32-8
N-methoxy-N-methyl-4-methyl-2-phenylpentanamide

: 75-16-1
methylmagnesium bromide

: 103392-12-7
5-Methyl-3-phenyl-2-hexanone

Guidance literature:: N-methoxy-N-methyl-4-methyl-2-phenylpentanamide; methylmagnesium bromide; In tetrahydrofuran; for 1h;

With hydrogenchloride; In tetrahydrofuran; water;

Reference yield:

: 103-82-2
phenylacetic acid

: 103392-12-7
5-Methyl-3-phenyl-2-hexanone

Guidance literature:: Multi-step reaction with 3 steps

1.1: lithium hexamethyldisilazane / tetrahydrofuran / 0 °C

2.1: oxalyl dichloride / N,N-dimethyl-formamide / dichloromethane / 1 h

2.2: 4 h

3.1: tetrahydrofuran / 1 h

With oxalyl dichloride; lithium hexamethyldisilazane; N,N-dimethyl-formamide; In tetrahydrofuran; dichloromethane;