Chlorooxoacetic acid 2-chloroallyl ester

Base Information

• Chemical Name: Chlorooxoacetic acid 2-chloroallyl ester
• CAS No.: 104142-66-7
• Molecular Formula: C5H4Cl2O3
• Molecular Weight: 182.98900
• Mol file: 104142-66-7.mol

Synonyms:2-Chloroallyl oxalochloride;Chlorooxoacetic acid 2-chloroallyl ester;Acetic acid,chlorooxo-,2-chloro-2-propenyl ester;

Chemical Property of Chlorooxoacetic acid 2-chloroallyl ester

Chemical Property:

• Refractive Index: n20/D1.466
• Flash Point: 93℃
• PSA: 43.37000
• Density: 1.371 g/mL at 25 °C
• LogP: 1.04750

Purity/Quality:

Mono(2-chloroallyl) oxalyl chloride 97% ^*data from reagent suppliers

Safty Information:

• Hazard Codes: C
• Statements: 22-34
• Safety Statements: 26-36/37/39-45

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Chlorooxoacetic acid 2-chloroallyl ester

There total 1 articles about Chlorooxoacetic acid 2-chloroallyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

2-chloroallyl alcohol (5976-47-6) + oxalyl dichloride (79-37-8) → 2-Chloroallyl oxalochloride (104142-66-7)

Guidance literature:

for 16h; Ambient temperature;

DOI:10.1021/jo00042a010

upstream raw materials:

2-chloroallyl alcohol

oxalyl dichloride

Refernces