Methyl 9H-fluorene-3-carboxylate

Base Information

Chemical Name:Methyl 9H-fluorene-3-carboxylate
CAS No.:104820-82-8
Molecular Formula:C15H12O2
Molecular Weight:224.25500
Hs Code.:
DSSTox Substance ID:DTXSID30516604
Nikkaji Number:J428.902A
Wikidata:Q82378090
Mol file:104820-82-8.mol

Synonyms:METHYL 9H-FLUORENE-3-CARBOXYLATE;104820-82-8;9H-Fluorene-3-carboxylic acid, methyl ester;SCHEMBL22524482;DTXSID30516604;AKOS025129127;CS-0440470

Suppliers and Price of Methyl 9H-fluorene-3-carboxylate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of Methyl 9H-fluorene-3-carboxylate

Chemical Property:

PSA：26.30000
LogP:3.04440
XLogP3:3.7
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:224.083729621
Heavy Atom Count:17
Complexity:299

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC(=O)C1=CC2=C(CC3=CC=CC=C32)C=C1

Technology Process of Methyl 9H-fluorene-3-carboxylate

There total 12 articles about Methyl 9H-fluorene-3-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 1263048-06-1
methyl 3-(2-bromophenyl)-4-methylbenzoate

: 104820-82-8
methyl fluorene-3-carboxylate

Guidance literature:: With N,N′-bis(2,6-diisopropylphenyl)imidazol-2-ylidene hydrochloride; palladium diacetate; potassium carbonate; In 1-methyl-pyrrolidin-2-one; at 130 ℃; for 4h; Inert atmosphere; Sealed tube;
DOI:10.1002/adsc.201000651

Reference yield: 77.0%

: (E)-methyl 6-methyl-2′-(pyrrolidin-1-yldiazenyl)-[1,1′-biphenyl]-3-carboxylate

: 104820-82-8
methyl fluorene-3-carboxylate

Guidance literature:: With trifluoroacetic acid; In toluene; at 100 ℃; for 1h;
DOI:10.1021/jo501640d

Reference yield:

: methyl 2'-methyl-6-(trifluoromethylsulfonyloxy)-[1,1'-biphenyl]-3-carboxylate

: 104820-82-8
methyl fluorene-3-carboxylate

Guidance literature:: With dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; potassium phosphate; palladium diacetate; In tetrahydrofuran; water; N,N-dimethyl-formamide; at 100 ℃; for 5h; Inert atmosphere;