Hydroxylamine, O,O'-1,2-ethanediylbis-, dihydrochloride

Base Information

• Chemical Name: Hydroxylamine, O,O'-1,2-ethanediylbis-, dihydrochloride
• CAS No.: 104845-83-2
• Molecular Formula: C2H8N2O2.2ClH
• Molecular Weight: 165.02

Synonyms:1,2-bis(aminooxy)ethane hydrochloride;1,2-bis-aminooxy-ethane,dihydrochloride;1,2-BIS(AMMONIOOXY)ETHANE DICHLORIDE;1,2-Bis-aminooxy-aethane,Dihydrochloride;1,2-diaminooxyethane bishydrochloride;1,2-Bis-aminooxy-aethane,Hydrochloride;

Chemical Property of Hydroxylamine, O,O'-1,2-ethanediylbis-, dihydrochloride

Chemical Property:

• PSA: 70.50000
• LogP: 0.96960

Purity/Quality:

98% ^*data from raw suppliers

1,2-BIS(AMMONIOOXY)ETHANE DICHLORIDE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Hydroxylamine, O,O'-1,2-ethanediylbis-, dihydrochloride

There total 3 articles about Hydroxylamine, O,O'-1,2-ethanediylbis-, dihydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.0%

N,N’-(ethylenedioxy)diphthalimide (6437-67-8) → O,O'-(ethane-1,2-diyl)bis(hydroxylamine) dihydrochloride (104845-83-2)

Guidance literature:

With hydrogenchloride; acetic acid; In water; at 100 ℃; for 6h; Inert atmosphere;

DOI:10.1021/acs.inorgchem.0c01156

Reference yield: 38.0%

C10H8BrNO3 → O,O'-(ethane-1,2-diyl)bis(hydroxylamine) dihydrochloride (104845-83-2)

Guidance literature:

C₁₀H₈BrNO₃; With hydrazine hydrate; at 20 ℃; for 12h;

With hydrogenchloride; In 1,4-dioxane; at 20 ℃; for 0.0833333h;

DOI:10.1002/chem.201800683

Reference yield:

→ O,O'-(ethane-1,2-diyl)bis(hydroxylamine) dihydrochloride (104845-83-2)

Guidance literature:

With hydrogenchloride;

upstream raw materials:

N,N’-(ethylenedioxy)diphthalimide

Downstream raw materials:

1,2-bis[N,N'-(2-mesitylsulphonyl)aminooxy]ethane

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